Bamboo charcoal cellulosic fiber and preparation method thereof
A cellulose fiber and cellulose technology is applied in the field of cellulose fiber containing bamboo charcoal and its preparation, which can solve the problems of fiber quality and performance influence, difficult recovery of chemical reagents, and reduced viscose spinnability, etc., and achieves the production process. Short, improved rheological properties, less toxic effect
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Embodiment 1
[0039]A kind of bamboo charcoal cellulose fiber, this fiber is obtained by spinning after bamboo charcoal pulp is mixed with the spinning dope that adopts ionic liquid to dissolve cellulose to make, and the content of its nano-bamboo charcoal is 5% of finished fiber weight, and described bamboo charcoal The specific indicators of cellulose fiber finished products include: dry breaking strength 2.5cN / dtex, dry breaking elongation 18%, dry breaking strength coefficient of variation CV 13%, defects ≤ 1mg / 100, bamboo charcoal content 5%, antibacterial rate > 99.9% , Ammonia adsorption > 50%, color fastness to washing 4-5.
[0040] The ionic liquid is a mixed ionic liquid of 1-butyl-methylimidazole chloride and 3-methyl-1-enphenylimidazolium chloride salt.
[0041] Described bamboo charcoal pulp is made from the raw material of following weight percent:
[0042] Bamboo Charcoal Powder 15%
[0043] Non-foaming dispersant 1%
[0044] Thickener 3%
[0045] Alkali 5%
[0046] The ...
Embodiment 2
[0060] A kind of bamboo charcoal cellulose fiber, this fiber is obtained by spinning after bamboo charcoal pulp is mixed with the spinning dope that adopts ionic liquid to dissolve cellulose to make, and the content of its nano-bamboo charcoal is 0.1% of finished fiber weight, and described bamboo charcoal The specific indicators of cellulose fiber finished products include: dry breaking strength 2.4cN / dtex, dry breaking elongation 20%, dry breaking strength coefficient of variation CV 14.5%, defect ≤ 1mg / 100, bamboo charcoal content 0.1%, antibacterial rate > 99.9% , Ammonia adsorption > 50%, color fastness to washing 4-5.
[0061] The ionic liquid is a mixed ionic liquid of 3-methyl-1-enphenylimidazolium chloride salt and 1-(2-hydroxyethyl)-3-methylimidazolium chloride salt.
[0062] Described bamboo charcoal pulp is made from the raw material of following weight percent:
[0063] Bamboo Charcoal Powder 5%
[0064] Non-foaming dispersant 1%
[0065] Thickener 1%
[0066]...
Embodiment 3
[0081] A kind of bamboo charcoal cellulose fiber, this fiber is obtained by spinning after bamboo charcoal pulp is mixed with the spinning stock solution that adopts ionic liquid to dissolve cellulose to make, and the content of its nano-bamboo charcoal is 10% of finished fiber weight, and described bamboo charcoal The specific indicators of cellulose fiber finished products include: dry breaking strength 2.42cN / dtex, dry breaking elongation 16%, dry breaking strength coefficient of variation CV 15%, defects ≤ 1mg / 100, bamboo charcoal content 10%, antibacterial rate > 99.9% , Ammonia adsorption > 50%, color fastness to washing 4-5.
[0082] The ionic liquid is a mixed ionic liquid of N-methyl-N-allylmorpholine chloride salt and 3-methyl-1-enphenylimidazolium chloride salt.
[0083] Described bamboo charcoal pulp is made from the raw material of following weight percent:
[0084] Bamboo Charcoal Powder 25%
[0085] Non-foaming dispersant 2%
[0086] Thickener 5%
[0087] Al...
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