Method for activating electroless copper-plated textile with nickel salt
A technology for electroless copper plating and textiles, applied in liquid chemical plating, metal material coating process, coating and other directions, can solve the problem of low catalytic activity, achieve the effect of simple solution composition, reduce precious metal pollution, and soft feel
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Embodiment 1
[0024] (1) Fabric coarsening: immerse the washed fabric (polyester brocade) in 20g / L NaOH roughening solution, raise the temperature to 60°C, keep it warm for 30min, then raise the temperature to 90°C and keep it for 60min, and wash it with 5% glacial acetic acid Wash with water, then wash with distilled water until neutral, and dry for later use.
[0025] (2) Polymer film formation: soak the fabric obtained in step (1) in a certain concentration of 18g / L chitosan solution, and use a uniform rolling machine (pressure: 1kg / cm 2 ) two dipping and two rolling, dry for later use.
[0026] (3) Activation treatment: immerse the fabric obtained in step (2) in 50g / L nickel sulfate solution at room temperature for 60min, then immerse in 10g / L sodium borohydride solution (pH=10.5) for 40min, and then clean it with distilled water and let dry.
[0027] (4) Electroless copper plating: Prepare the composition of electroless copper plating solution: nickel sulfate 6g / L, copper sulfate 35g...
Embodiment 2
[0030] (1) Fabric roughening: immerse the washed fabric (nylon cloth) in 15g / L NaOH roughening solution, raise the temperature to 60°C, keep it warm for 30 minutes, then raise the temperature to 90°C and keep it warm for 60 minutes, and neutralize it with 5% glacial acetic acid Wash with water, then wash with distilled water until neutral, and dry for later use.
[0031] (2) Polymer film formation: soak the fabric obtained in step (1) in 15g / L chitosan solution, and use a uniform paddle (pressure: 1kg / cm 2 ) two dipping and two rolling, dry for later use.
[0032] (3) Activation treatment: immerse the fabric obtained in step (2) in 40g / L nickel sulfate solution at room temperature for 60min, then immerse in 8g / L sodium borohydride solution (pH=10) for 35min, and then clean it with distilled water and let dry.
[0033] (4) Electroless copper plating: Prepare the composition of electroless copper plating solution: nickel sulfate 8g / L, copper sulfate 40g / L, hydrazine hydrate 30...
Embodiment 3
[0036] (1) Fabric roughening: immerse the washed fabric (polyester cloth) in 25g / L NaOH roughening solution, raise the temperature to 60°C, keep it warm for 30 minutes, then raise the temperature to 90°C and keep it warm for 60 minutes, and neutralize it with 5% glacial acetic acid Wash with water, then wash with distilled water until neutral, and dry for later use.
[0037] (2) Polymer film formation: soak the fabric obtained in step (1) in a certain concentration of 20g / L chitosan solution, and use a uniform rolling machine (pressure: 1kg / cm 2 ) two dipping and two rolling, dry for later use.
[0038] (3) Activation treatment: immerse the fabric obtained in step (2) in 60g / L nickel sulfate solution at room temperature for 50min, then immerse in 12g / L sodium borohydride solution (pH=11) for 45min, and then clean it with distilled water and let dry.
[0039](4) Electroless copper plating: Prepare the composition of electroless copper plating solution: nickel sulfate 5g / L, co...
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