High voltage electrolyte for hybrid super tantalum capacitor and preparation method thereof
A tantalum capacitor and hybrid technology, applied in the field of high-voltage electrolytes for hybrid super tantalum capacitors and their preparation
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Embodiment 1
[0059] 1. Preparation of impregnated electrolyte
[0060] a) Weigh 5g of ethylene glycol-methyl ether and 5g of ethylene glycol-butyl ether and mix evenly, then add 10g of N,N-dimethylformamide and 5g of dimethyl sulfoxide, mix and stir at room temperature, and slowly heat up to 80°C;
[0061] b), then weigh 4.2g of 1-propyl-3-n-butylimidazolium tetrafluoroborate, add it at 80°C, raise the temperature to 110°C, stir and keep it warm for 1h, and then cool to room temperature to obtain Mix liquid A;
[0062] c) Weigh VOSO 4 ·5H 2 O0.8g, it is dissolved in 44g deionized water, then measures the concentrated sulfuric acid 26g, in the process of constantly stirring, it is slowly added dropwise to VOSO 4 ·5H 2 In the O aqueous solution, the pH value is controlled at about 2.5 to prepare mixed B liquid;
[0063] d) Add the mixed liquid A into the mixed liquid B while stirring continuously, and the electrolyte solution for impregnation can be obtained after stirring evenly.
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Embodiment 2
[0071] 1. Preparation of impregnated electrolyte
[0072] a) Weigh 2.5g of polyethylene glycol and 2.5g of ethylene glycol-butyl ether and mix evenly, then add 12.5g of N,N-dimethylformamide and 37.5g of N-methylpyrrolidone, mix and stir at room temperature, and Slowly heat up to 80°C;
[0073] b) Then weigh 1 g of 1-n-butyl-3-methylimidazolium tetrafluoroborate, add it at 80°C, raise the temperature to 110°C, stir and keep it warm for 1h, and then cool to room temperature to obtain a mixed A liquid;
[0074] c) Weigh CuSO 4 ·5H 2 0.5g, it is dissolved in 23.5g deionized water, then measures 20g of concentrated sulfuric acid, in the process of constant stirring, it is slowly added dropwise to CuSO 4 ·5H 2 In the O aqueous solution, the pH value is controlled at about 2.0 to prepare mixed B liquid;
[0075] d) Add the mixed liquid A into the mixed liquid B while stirring continuously, and the electrolyte solution for impregnation can be obtained after stirring evenly.
...
Embodiment 3
[0083] 1. Preparation of impregnated electrolyte
[0084] a) Weigh 10g of ethylene glycol and 10g of ethylene glycol-butyl ether and mix evenly, then add 10g of dimethyl sulfoxide, mix and stir at room temperature, and slowly heat up to 80°C;
[0085] b) Then weigh 1g of 1-propyl-3-ethylimidazolium tetrafluoroborate, add it at 80°C, raise the temperature to 110°C, stir and keep it warm for 1h, and then cool to room temperature to prepare Mixture A liquid;
[0086] c) Weigh VOSO 4 ·5H 2 O1.5g, dissolve it in 35.5g deionized water, then measure 32g of concentrated sulfuric acid, slowly add it dropwise to VOSO in the process of constant stirring 4 ·5H 2 In the O aqueous solution, the pH value is controlled at about 2.0 to prepare mixed B liquid;
[0087] d) Add the mixed liquid A into the mixed liquid B while stirring continuously, and the electrolyte solution for impregnation can be obtained after stirring evenly.
[0088] 2. Preparation of gel electrolyte
[0089] a) Wei...
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