A kind of preparation method and application of high-strength super heat-resistant MC nylon composite material
A nylon composite material, super heat-resistant technology, applied in the direction of coating, etc., can solve the problems of poor dimensional stability, high pressure required for molding, difficult to heat evenly, etc., and achieve the effect of improving performance indicators, improving heat resistance and water absorption
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Embodiment 1
[0028] A kind of preparation method of high-strength super heat-resistant MC nylon composite material is carried out according to the following steps:
[0029] 1) According to the parts by weight, put 2000 parts of caprolactam into the melting tank, heat it to 125 degrees, start the vacuum pump to evacuate to 0.04Mpa, after 8 minutes of vacuuming, turn off the vacuum pump, add 3 parts of sodium hydroxide, and evacuate for 8 minutes. The temperature is maintained at 140 degrees;
[0030] 2) Send 50 parts of thermotropic crystallization polymer, 15 parts of vinyl triperoxy-tert-butylsilane and 120 parts of short fibers into a double paddle reverse high-speed shearing machine, shear and disperse for 0.8 hours, and obtain thermotropic crystallization polymer short fiber;
[0031] 3) Put the pyrogenic crystalline polymer short fibers into the melting kettle described in step (1), and shake the melting kettle for 15 laps;
[0032] 4) Add 8 parts of toluene diisocyanate to the melt...
Embodiment 2
[0042] A kind of preparation method of high-strength super heat-resistant MC nylon composite material is carried out according to the following steps:
[0043] 1) According to the parts by weight, put 2000 parts of caprolactam into the melting tank, heat it to 125 degrees, start the vacuum pump to evacuate to 0.04Mpa, after 8 minutes of vacuuming, turn off the vacuum pump, add 3 parts of sodium hydroxide, and evacuate for 8 minutes. The temperature is maintained at 140 degrees;
[0044] 2) 50 parts of thermal crystallization polymers, 30 parts of elm bark fibers, 15 parts of vinyl triperoxy tert-butyl silane and 120 parts of short fibers are sent into double-blade reverse high-speed shearing machine, and sheared and dispersed for 0.8 hours to obtain thermotropic crystallization polymer short fibers;
[0045] 3) Put the pyrogenic crystalline polymer short fibers into the melting kettle described in step (1), and shake the melting kettle for 15 laps;
[0046] 4) Add 8 parts of...
Embodiment 3
[0056] A kind of preparation method of high-strength super heat-resistant MC nylon composite material is carried out according to the following steps:
[0057] 1) According to the parts by weight, put 2000 parts of caprolactam into the melting tank, heat to 120 degrees, start the vacuum pump to evacuate to 0.01Mpa, after 10 minutes of vacuuming, turn off the vacuum pump, add 2 parts of sodium hydroxide, and evacuate for 10 minutes. The temperature is maintained at 135 degrees;
[0058] 2) Send 10 parts of thermotropic crystallization polymer, 10 parts of γ-mercaptopropyltriethoxysilane and 50 parts of short fibers into double-blade reverse high-speed shearing machine, and shear and disperse for 0.5 hours to obtain thermotropic crystallization polymer short fibre;
[0059] (3) Put the thermal crystallization polymer short fiber into the melting kettle described in step (1), and shake the melting kettle for 5 turns;
[0060] 4) Add 6 parts of diphenylmethane diisocyanate into ...
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