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Chuju chrysanthemum extract, solid beverage, lozenge and food additive and preparation method thereof

A technology for food additives and solid beverages, which is applied to Chu chrysanthemum extracts, lozenges and food additives and their preparation, and the field of solid beverages, can solve the problem that it is difficult to exert the health care function of chrysanthemum, the content of chrysanthemum active ingredients is low, and the loss of chrysanthemum active ingredients is large. and other problems, to achieve the effect of low cost, low production cost and low energy consumption of equipment

Inactive Publication Date: 2015-12-30
NANJING UNIVERSITY OF TRADITIONAL CHINESE MEDICINE
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The main component of the existing chrysanthemum crystal series products is sucrose, and the active ingredient content of chrysanthemum is very low, so it is difficult to exert the health care function of chrysanthemum; The loss of ingredients is large; in addition, the existing chrysanthemum crystal mainly contains sucrose, which is not suitable for children, obese people and diabetic patients

Method used

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  • Chuju chrysanthemum extract, solid beverage, lozenge and food additive and preparation method thereof
  • Chuju chrysanthemum extract, solid beverage, lozenge and food additive and preparation method thereof
  • Chuju chrysanthemum extract, solid beverage, lozenge and food additive and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0031] The volatile oil of Chu chrysanthemum was extracted by steam distillation method combined with membrane separation method. The specific method is: take 100kg of Chu chrysanthemum, pulverize it through a 40-mesh sieve, add water 12 times the weight of Chu chrysanthemum, enter into a multi-functional extraction tank, perform steam distillation to extract volatile oil, distill for 4 hours, collect Chu chrysanthemum dregs and separate oil and water The volatile oil and oil-water mixture separated by the device. About 80 ml of volatile oil were obtained, and the yield was 0.8%. The oil-water mixture was passed through a polysulfone membrane with a molecular weight cut-off of 140,000 Daltons to implement oil-water separation. The operating pressure was 0.10 MPa and the operating temperature was 60°C to obtain about 10 ml of volatile oil. The two volatile oils obtained were combined to obtain the total volatile oil of Chuju.

[0032] Inclusion of volatile oil with β-CD: the ...

Embodiment 2

[0036] Example 2 Verification of volatile oil β-cyclodextrin inclusion complex

[0037] The volatile oil β-cyclodextrin inclusion complex was verified by TLC and DSC.

[0038] (1) Thin-layer chromatography (TLC)

[0039] Dissolve β-CD, blank β-CD inclusion complex, volatile oil β-CD inclusion complex and Chuju total volatile oil in cyclohexane, respectively, and spot them on a silica gel G thin-layer plate with cyclohexane:hexyl acetate (17:3) is the developing agent for chromatography. After the chromatography, spray with 5% vanillin-concentrated sulfuric acid and bake at 105°C for 10 min to develop color. see the results figure 1 .

[0040] On the thin layer chromatogram ( figure 1 ), β-CD has no spots, blank β-CD inclusion complex has no spots, volatile oil β-CD inclusion complex and Chuju total volatile oil have the same spots, indicating the formation of volatile oil β-CD inclusion complex, and β-CD inclusion complex The composition of volatile oil did not change be...

Embodiment 3

[0046] Take 20kg of sucrose, pulverize it through an 80-mesh sieve, add 2kg of Chu chrysanthemum extract, mix evenly, and prepare spherical or spherical-like granules with a 20-40 mesh sieve by centrifugal flow granulation. BZJ-360M coating granulator ( The 15th Institute of China Academy of Launch Vehicle Technology, Beijing Tianming High-tech Development Company) technical parameters: main engine speed 80~120r / min, shotcrete pump speed 5~50r / min, powder feeder speed 10~100r / min, jet pressure 0.10~2.5MPa, blast volume 5~15L / min, blast temperature 50~70℃, particle temperature 30~60℃, use 70% concentration of medicinal ethanol aqueous solution as binder to prepare spherical or spherical shape particles.

[0047] A total of 21.5kg of 20-40 mesh granules were obtained, with a yield of 96%.

[0048] Take the above-mentioned granules and pack them in small aluminum-plastic packaging bags, each bag of 4.0 g, to obtain a Chuju solid drink, which can be taken by adding 150-250 ml of ...

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Abstract

The invention provides chrysanthemum chrysanthemum extract, solid beverage, buccal tablet and food additive and preparation method thereof ， It involves the field of functional food. The preparation method of the chrysanthemum chrysanthemum extract comprises the following steps: (1) extracting the volatile oil of the chrysanthemum chrysanthemum; (2) decocting the residual chrysanthemum chrysanthemum with water, taking the filtrate, concentrating, and spray drying to obtain a spray-dried powder; (3) The chrysanthemum chrysanthemum extract is obtained after mixing the volatile oil with the spray-dried powder. The present invention also claims to protect the chrysanthemum chrysanthemum extract prepared by the method, the solid drink, buccal tablet and food additive with the chrysanthemum chrysanthemum extract as active ingredients. The method for preparing the chrysanthemum chrysanthemum extract of the present invention can safely and efficiently extract the active ingredients in the chrysanthemum chrysanthemum flower, and the cost is low. The chrysanthemum chrysanthemum extract prepared by the present invention, the solid drink, buccal tablet and food additive with the chrysanthemum chrysanthemum extract as an active ingredient contain a large amount of active ingredients of chrysanthemum chrysanthemum, are safe, and are not only suitable for ordinary healthy people, but also suitable for children , obesity and diabetes.

Description

technical field [0001] The invention relates to the field of functional foods, in particular to chrysanthemum chrysanthemum extracts, solid beverages, buccal tablets, food additives and preparation methods thereof. Background technique [0002] Chu chrysanthemum is the dry flower head of Chrysanthemum morifolium Ramat. Chuzhou chrysanthemum is commonly known as chamomile and white chrysanthemum. It is a traditional and precious specialty in Chuzhou City, Anhui Province. It has a cultivation history of more than 2,000 years. It was accepted as a tribute in the Qing Dynasty, so it is also called "Chuzhou Tribute Chrysanthemum". Chu chrysanthemum has huge golden stamens and crystal clear jade-white petals. It is one of the four major medicinal materials in Anhui Province, and its health care value ranks first among the four famous chrysanthemums. Chu chrysanthemum has the functions of dispelling wind and clearing heat, clearing liver and improving eyesight. It is mainly used t...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): A23L2/39A23L1/29A23L1/30C11B9/02A23L33/00
CPCA23L2/39A23L33/00A23L33/10A23V2002/00C11B9/022C11B9/027A23V2250/21A23V2200/30A23V2200/332A23V2200/328
Inventor 郭立玮朱华旭刘陶世付廷明沈强
Owner NANJING UNIVERSITY OF TRADITIONAL CHINESE MEDICINE
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