Environment-friendly vegetable protein based efficient water and fertilizer slow/controlled-release material
A technology of controlled release material and vegetable protein, which is applied in the field of plant protein-based high-efficiency water and fertilizer slow and controlled release materials, can solve the problems of poor slow and controlled release effect, high price, environmental pollution, etc., achieve excellent slow and controlled release characteristics, improve The effect of water and fertilizer utilization
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Embodiment 1
[0025] Embodiment 1: Preparation of thermoplastic vegetable protein
[0026] Crush one or more of soybean meal, peanut meal, rapeseed meal, cottonseed meal, sunflower meal, tea seed meal, rice bran, bran (vegetable protein raw material) after impurity removal, and add 10 times the weight of vegetable protein NaOH solution with a pH of 8.0, treated at 50°C for 1 hour, filtered, centrifuged, and insoluble impurities removed, the filtrate was adjusted to pH 4.5 with sulfuric acid to cause protein coagulation and precipitation, separated, washed, and neutralized to obtain plant purified protein; plant purified Add urea buffer solution 30 times the weight of protein and plant purified protein into the reaction kettle, stir at 60°C for 30 min under the condition of blowing nitrogen, then add mercaptoethanol equivalent to the weight of plant purified protein to react for 1 hour, and the protein molecules are fully dissolved in the solution Stretch, then add initiator and graftin...
Embodiment 2
[0028] Get 30 parts of thermoplastic vegetable proteins prepared by Example 1, 60 parts of ethylene / vinyl acetate copolymers (EVA), 7 parts of undecenyl succinic anhydride, 5 parts of benzoyl peroxide, 5 parts of sodium carbonate, 5 parts of paraffin wax were mixed in a high-speed mixer for 30 min, then melt-blended and extruded in a twin-screw extruder with a melt-blending temperature of 110°C, a die temperature of 120°C, and a screw speed of 20 rpm; Cooling in air, granulation and coarse crushing to prepare the high-efficiency water and fertilizer slow-controlled release material of the present invention, wherein the water and fertilizer refer to water-soluble chemical fertilizers.
Embodiment 3
[0030]Get 60 parts of thermoplastic vegetable proteins prepared in Example 1, 40 parts of ethylene / ethyl acrylate copolymer (EEA), 6 parts of dodecenyl succinate, 3 parts of lauroyl peroxide, 3 parts of sodium bicarbonate by weight. 3 parts of stearic acid and 3 parts of stearic acid were mixed in a high-speed mixer for 25 min, melt blended and extruded in a twin-screw extruder with a melt blending temperature of 120 ° C, a die temperature of 130 ° C, and a screw speed of 30 rpm ; Cooling in natural air, granulation, coarse crushing to prepare the high-efficiency water and fertilizer slow-controlled release material of the present invention.
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