A special self-repairing biodegradable sealing grease for shield machine main bearing and preparation method thereof
A biodegradable and self-healing technology, applied in lubricating compositions and other directions, can solve problems such as inability to actively respond to changes in the underground environment, harsh and complex underground environments, and achieve excellent pumping performance, tight structure, and not easy to absorb water.
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Embodiment 1
[0017] In embodiment one, the following components are used to prepare the sealant of the present invention, wherein the percentage is based on the total weight of the sealant: the sebacate of 38% by weight is selected as the biodegradable base oil, 5% by weight of guar gum as a biodegradable tackifier, 9% by weight of coniferous wood fiber as a biodegradable thickener, 6% by weight of sodium hydroxymethyl cellulose as a self-repairing stabilizer, 5% by weight of carbon black as an inorganic solid lubricant and 37% by weight of barium sulfate and talc as fillers.
[0018] The preparation method is as follows: put sebacate and guar gum into the reaction kettle, stir and heat up to 50-60°C, then add coniferous wood fiber, sodium hydroxymethyl cellulose, carbon black, and control the temperature at 50-60°C. Stir at 60°C for 30 minutes, finally add barium sulfate and talcum powder and stir and mix for 90 minutes.
Embodiment 2
[0020] In embodiment two, the following components are used to prepare the sealant of the present invention, wherein the percentage is based on the total weight of the sealant: the sebacate of 40% by weight is selected as the biodegradable base oil, The flax gum of 8% by weight is used as biodegradable tackifier, the coniferous wood fiber of 12% by weight is used as biodegradable thickener, the sodium hydroxymethyl cellulose of 7% by weight is used as self-repairing stabilizer, 7% by weight % by weight of white carbon black as an inorganic solid lubricant and 26% by weight of kaolin and heavy calcium as fillers.
[0021] The preparation method is as follows: put sebacate and flax gum into the reaction kettle, stir and heat up to 50-60°C, then add coniferous wood fiber, sodium hydroxymethyl cellulose, white carbon black, and control the temperature at 50-60°C. Stir at 60°C for 30 minutes, and finally add kaolin and heavy calcium and stir and mix for 90 minutes.
Embodiment 3
[0023] In Example 3, the following components are used to prepare the sealing grease of the present invention, wherein the percentage is based on the total weight of the sealing grease: select 39% by weight of azelaic acid ester as the biodegradable base oil, 10% by weight of gelatin as a biodegradable thickener, 11% by weight of coniferous wood fiber as a biodegradable thickener, 7% by weight of sodium hydroxymethylcellulose as a self-healing stabilizer, 7% by weight White carbon black in weight percentage is used as inorganic solid lubricant and 26 weight percent of barium sulfate, kaolin and diatomaceous earth are used as fillers.
[0024] The preparation method is as follows: put azelaic acid ester and gelatin into the reaction kettle, stir and heat up to 50-60°C, add coniferous wood fiber, sodium hydroxymethyl cellulose, white carbon black, and control the temperature at 50-60°C Stir for 30 minutes, add barium sulfate, kaolin and diatomaceous earth and stir and mix for 90...
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Abstract
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