Composite functional infrared reflective engineering machinery powder coating and its production process
An infrared reflective pigment and infrared reflective technology, applied in the production of powder coatings, reflective/signal coatings, bulk chemicals, etc., can solve problems such as not very easy, numerous devices, cumbersome production processes, etc. Baking temperature, the effect of reducing production costs
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Embodiment 1
[0045] Preparation of polyester / acrylic resin composite 1: It is prepared by mixing polyester resin and acrylic resin in a weight ratio of 7:3, and reacting in a high-temperature reactor at 150° C. for 1 hour.
[0046] Preparation of epoxy-modified acrylic resin: using methyl methacrylate, acrylic acid, octyl acrylate, styrene, hydroxypropyl acrylate, trimethylolpropane triacrylate as monomers, benzoyl peroxide as initiator, E-44 epoxy resin is used as modifier and polymerized.
[0047] Preparation of nanocomposite cross-linking agent: 4,5-imidazole dicarboxylic acid and benzimidazole-5,6-dicarboxylic acid as sensitized organic ligands, grafted onto mesoporous SiO through covalent bonds 2 On the nanoparticles, a nanocomposite cross-linking agent is prepared.
[0048] The infrared reflective pigment is rutile nano-titanium dioxide, and the polyester resin is 9855 polyester resin supplied by Baotian New Materials.
[0049] The raw material components of the powder coating are ...
Embodiment 2
[0053] This embodiment is basically the same as Embodiment 1, and its difference is:
[0054] To prepare polyester / acrylic composite 2, react for 1.5 hours.
[0055] The method of CN103467714A is adopted to prepare high hydroxyl polyester resin.
[0056] The method of CN102795663A is adopted to prepare nanoscale titanium dioxide-coated mica powder.
[0057] The crosslinking agent is trimethylolpropane.
[0058] In addition, the additives are different, see Table 1 for details.
Embodiment 3
[0060]This embodiment is basically the same as Embodiment 1, the difference is that the additives are different, the temperature of the supercritical fluid tank is set to 120 ° C, after heating to the set temperature, the temperature is kept constant for 5 minutes, and the rotation speed of the shearing element is 150 rpm / min, the shear mixing time is 10 minutes.
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