A preparation method of adsorption visible light catalytic material for air pollution control
A catalytic material, air pollution technology, applied in chemical instruments and methods, physical/chemical process catalysts, separation methods, etc., can solve problems such as poor adsorption performance, low efficiency, and unfavorable promotion, and achieve improved mechanical strength and good adsorption. , the effect of large specific surface area
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Embodiment 1
[0021] (1) Proportion coal gangue, tourmaline and asphalt powder with a particle size of 200 meshes according to the weight ratio of coal gangue: tourmaline: asphalt powder = 0.8:0.05:0.15, and fully mix them to obtain material A.
[0022] (2) At room temperature, mix tetra-n-butyl titanate and absolute ethanol at a volume ratio of 1:1, and stir for 0.5 h to obtain a uniform and transparent yellow solution B.
[0023] (3) Mix the material A and the yellow solution B at a mass volume ratio of 1:3, age for 24 hours, heat up to 650°C for carbonization for 6 hours under the condition of carbon dioxide gas with a flow rate of 200mL / min, and cool to room temperature to prepare Get material C.
[0024] (4) Mix material C and sodium tungstate aqueous solution according to the mass volume ratio (w / v) of 10% (the weight ratio of material C and sodium tungstate is 0.95:0.05), ultrasonically oscillate for 4 hours, then wash and dry, nitrogen atmosphere Activation at 400°C for 2 hours, co...
Embodiment 2
[0027] (1) Proportion coal gangue, tourmaline and asphalt powder with a particle size of 200 meshes according to the weight ratio of gangue: tourmaline: asphalt powder = 0.85:0.03:0.12, and fully mix them to obtain material A.
[0028] (2) At room temperature, mix tetra-n-butyl titanate and absolute ethanol at a volume ratio of 1:1, and stir for 0.5 h to obtain a uniform and transparent yellow solution B.
[0029] (3) Mix material A and yellow solution B at a mass volume ratio of 1:3, age for 12 hours, raise the temperature to 550°C for carbonization for 6 hours under the condition of carbon dioxide gas with a flow rate of 200mL / min, and cool to room temperature to prepare Get material C.
[0030] (4) Fully mix material C and sodium tungstate aqueous solution according to the mass volume ratio (w / v) of 10% (the weight ratio of material C and sodium tungstate is 0.93:0.07), ultrasonically oscillate for 4 hours, then wash and dry, nitrogen atmosphere Activation at 500°C for 2 h...
Embodiment 3
[0033] (1) Proportion coal gangue, tourmaline and asphalt powder with a particle size of 200 meshes according to the weight ratio of gangue: tourmaline: asphalt powder = 0.7:0.08:0.22, and fully mix to obtain material A.
[0034] (2) At room temperature, mix tetra-n-butyl titanate and absolute ethanol at a volume ratio of 1:1, and stir for 0.5 h to obtain a uniform and transparent yellow solution B.
[0035] (3) Mix the material A and the yellow solution B at a mass volume ratio of 1:4, age for 24 hours, heat up to 600°C for carbonization for 8 hours under the condition of carbon dioxide gas with a flow rate of 200mL / min, and cool to room temperature to prepare Get material C.
[0036](4) Mix material C and sodium tungstate aqueous solution according to the mass volume ratio (w / v) of 10% (the weight ratio of material C and sodium tungstate is 0.95:0.05), ultrasonically oscillate for 4 hours, then wash and dry, nitrogen atmosphere Activation at 500°C for 2 hours, cooling to ro...
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