Production method of microcrystalline glass-ceramic composite brick

A technology of glass-ceramic ceramics and a production method, which is applied in the field of architectural ceramics, can solve the problem of insufficient layering of the decorative surface, achieve the level of artistic aesthetics and improve decorative performance, rich in color changes, and improve the level of artistic aesthetics and decorative performance Effect

Active Publication Date: 2015-01-28
HANGZHOU NABEL CERAMIC
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] In order to solve the problem that the layering of the decorative surface of the existing glass-ceramic composite bricks is not rich enough, the present invention introduces high-calcium raw materials and uses the crystal nucleating agent in reverse to control the crystallization area and transparency and / or translucency. The staggered distribution of regions provides a production method for glass-ceramic composite bricks with rich layers and good decorative effects

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] (1) Preparation of high calcium raw material: prepare 30~80 mesh wollastonite, for subsequent use;

[0028] (2) Preparation of low-viscosity glass frit and high-viscosity glass frit: The conventional glass frit preparation process is adopted respectively, and quartz, feldspar and chemical raw materials are selected, and through batching, melting, water quenching, drying, crushing, Through sieving, grading and other procedures, low-viscosity glass frit and high-viscosity glass frit particles with a particle size of 8-20 meshes are prepared for use;

[0029] In order to match the glass-ceramic composite brick substrate in terms of firing temperature and thermal expansion properties, the chemical composition range of the low-viscosity glass frit is (parts by weight): SiO 2 : 45%, Al 2 O 3 : 12%, CaO: 14%, MgO: 6%, K 2 O: 1.5%, Na 2 O: 2%, ZrO 2 : 3%, BaO: 4%, B 2 O 3 : 3%, Li 2 O: 0.2%, impurities and appropriate proportions of clarifying agent and crystal nucleati...

Embodiment 2

[0035] (1) the preparation of high calcium raw material: prepare 30~80 purpose limestone and calcite respectively and mix, and the ratio (weight part) of limestone and calcite is 1:1, for subsequent use;

[0036] (2) Preparation of low-viscosity glass frit and high-viscosity glass frit: The conventional glass frit preparation process is adopted respectively, and quartz, feldspar and chemical raw materials are selected, and through batching, melting, water quenching, drying, crushing, Through sieving, grading and other procedures, low-viscosity glass frit and high-viscosity glass frit particles with a particle size of 6-20 meshes are prepared, which are ready for use;

[0037] In order to match the glass-ceramic composite brick substrate in terms of firing temperature and thermal expansion properties, the chemical composition range of the low-viscosity glass frit is (parts by weight): SiO 2 : 41%, Al 2 O 3 : 14%, CaO: 10%, MgO: 5%, K 2 O: 3%, Na 2 O: 4%, ZrO 2 : 2%, BaO: 6...

Embodiment 3

[0043] (1) Preparation of high calcium raw material: The chemical composition of preparing 30~80 meshes is (parts by weight): SiO 2 : 46%, Al 2 O 3 : 8%, CaO: 35%, K 2 O: 3%, Na 2 O: 1.5%, BaO: 3.5%, the balance is high calcium frit with auxiliary materials and impurities, spare;

[0044] (2) Preparation of low-viscosity glass frit and high-viscosity glass frit: The conventional glass frit preparation process is adopted respectively, and quartz, feldspar and chemical raw materials are selected, and through batching, melting, water quenching, drying, crushing, Through sieving, grading and other processes, low-viscosity glass frit and high-viscosity glass frit particles with a particle size of 10-30 meshes are prepared, which are ready for use;

[0045]In order to match the glass-ceramic composite brick substrate in terms of firing temperature and thermal expansion properties, the chemical composition range of the low-viscosity glass frit is (parts by weight): SiO 2 : 48%, ...

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PUM

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Abstract

The invention discloses a production method of a microcrystalline glass-ceramic composite brick. The production method comprises the following steps: (1) preparing a high-calcium raw material; (2) preparing a low-viscosity glass frit and a high-viscosity glass frit; (3) preparing powder of a green microcrystalline glass-ceramic composite brick through a conventional method; (4) preparing a microcrystalline glass-ceramic composite brick substrate from the powder of the green microcrystalline glass-ceramic composite brick prepared by the step (3) through a conventional method; (5) preparing a microcrystalline glass-ceramic composite brick; and (6) post-processing. The microcrystalline glass-ceramic composite brick prepared by the production method disclosed by the invention, through staggered distribution of crystallization regions and transparent and/or semitransparent regions, changes an original monotonous texture that has only crystallization patterns on the entire surface, and the brick is richer in pattern layering sense and better in decoration effect; the production method disclosed by the invention is lower in sintering temperature, shorter in sintering cycle, and capable of greatly reducing energy consumption, relieving emission and saving manufacturing cost; and the prepared composite brick has fewer surface pores, good anti-fouling performance and high wear resistance.

Description

technical field [0001] The invention relates to the technical field of building ceramics, in particular to a production method of a glass-ceramic composite brick. Background technique [0002] Glass-ceramics has excellent properties such as compact structure, wear resistance, corrosion resistance, high mechanical strength, and strong weathering resistance, and can be used as high-grade building decoration materials. However, the whole body of glass-ceramics has high energy consumption, high pollution and high cost during manufacture; while glass-ceramics is used as the surface finish layer, or a mixture of glass-ceramics and ceramics is used as the surface finish layer, and then ordinary ceramics As the bottom support layer, made of glass-ceramic composite bricks is conducive to greatly reducing energy consumption, reducing emissions, saving manufacturing costs, and is easy for large-scale industrial production. [0003] The basic production process of glass-ceramic composi...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B32B17/06B32B18/00C03C10/00
CPCB32B17/06B32B18/00C03C10/00
Inventor 赵明夏昌奎彭西洋郁建荣王磊郭弟
Owner HANGZHOU NABEL CERAMIC
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