Method for preparing polyether glycol with rape stalks as raw materials
A technology of polyether polyol and rape straw, which is applied in the field of polymer chemistry research, can solve the problems of complex operation, raw material modification, and many side reactions, and achieve the effect of simple process, mild conditions, and low cost
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[0031] Example 1
[0032] A preparation method of polyether polyol using rape straw as a raw material, specifically comprising the following steps:
[0033] (1) Crush the rape stalks to 30 meshes, and bake them at 120°C for 1 hour to obtain straw powder;
[0034] (2) According to the ratio of liquefaction agent:catalyst mass ratio of 100:5, add liquefaction agent and catalyst to a four-necked flask equipped with mechanical stirrer, condenser and thermometer, and heat up to 100 while stirring. ℃, get the mixed solution;
[0035] The liquefaction agent is a mixture of glycerol and polyethylene glycol with a molecular weight of 400 g / mol in a mass ratio of 3:9;
[0036] The catalyst is sulfuric acid;
[0037] (3) Add the straw powder obtained in step (1) to the mixed liquid obtained in step (2), continue to heat up to 120°C for 120 min, and then naturally lower to room temperature to obtain a reaction liquid;
[0038] The amount of straw powder mentioned above is calculated by mass ratio...
Example Embodiment
[0044] Example 2
[0045] A preparation method of polyether polyol using rape straw as a raw material, specifically comprising the following steps:
[0046] (1) Crush the rape straw to 30 mesh, and bake it at 120℃ for 1 h to obtain straw powder;
[0047] (2) According to the ratio of liquefaction agent:catalyst mass ratio of 100:3, add liquefaction agent and catalyst into a four-necked flask equipped with mechanical stirrer, condenser and thermometer, and heat up to 140 while stirring. ℃, get the mixed solution;
[0048] The liquefaction agent is a mixture of glycerol and polyethylene glycol with a molecular weight of 400 g / mol in a mass ratio of 3:3;
[0049] The catalyst is sulfuric acid;
[0050] (3) Add the straw powder obtained in step (1) to the mixed solution obtained in step (2), continue to heat up to 160°C for 140 min, and then naturally lower to room temperature to obtain a reaction solution;
[0051] The above-mentioned amount of straw powder is calculated by mass ratio, s...
Example Embodiment
[0057] Example 3
[0058] A preparation method of polyether polyol using rape straw as a raw material, specifically comprising the following steps:
[0059] (1) Crush the rape straw to 30 mesh, and bake it at 120℃ for 1 h to obtain straw powder;
[0060] (2) According to the ratio of liquefaction agent:catalyst mass ratio of 100:1, add liquefaction agent and catalyst to a four-necked flask equipped with mechanical stirrer, condenser and thermometer, and heat up to 150 while stirring. ℃, get the mixed solution;
[0061] The liquefaction agent is a mixture of glycerol and polyethylene glycol with a molecular weight of 400 g / mol in a mass ratio of 3:1;
[0062] The catalyst is sulfuric acid;
[0063] (3) Add the straw powder obtained in step (1) to the mixed solution obtained in step (2), continue to raise the temperature to 170°C for 60 min, and then naturally lower to room temperature to obtain a reaction solution;
[0064] The amount of straw powder is calculated by mass ratio, straw ...
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