Phase-change energy-storage dual-limit temperature adjustment mortar and preparation method thereof
A technology of phase change energy storage and phase change temperature, which is applied in the field of building materials, can solve the problems of high cost of phase change microcapsules, loss of energy storage and temperature regulation function, and difficulty in long-term performance of energy storage and temperature regulation effects of phase change mortar, etc. question
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Embodiment 1
[0086] Step 1: Prepare phase change microcapsules with a phase change temperature of 18-20 degrees Celsius
[0087] 10 parts of polystyrene and 10 parts of butyl stearate are dissolved in 80 parts of dichloromethane, and the above-mentioned oil phase solution is slowly dripped into 600 parts of 1% aqueous sodium lauryl sulfate solution in an emulsifier with Stir at a speed of 2800r / min for 30 minutes, then reduce the speed to 500r / min, heat the emulsion until the temperature reaches 35-40 degrees Celsius, continue stirring for 2 hours, filter, wash, and dry to obtain polystyrene capsule wall—stearic acid Butyl ester capsule core phase change microcapsules have a phase change temperature of 19.5 degrees Celsius and a latent heat of phase change of 84 kJ / kg as tested by DSC, and an average particle size of 38 microns as tested by a laser particle size analyzer.
[0088] Step 2: Prepare expanded perlite shaped phase change particles with a phase change temperature of 26-28 degree...
Embodiment 2
[0093] Step 1: Prepare phase change microcapsules with a phase change temperature of 18-20 degrees Celsius
[0094] Dissolve 10 parts of polysulfone and 12 parts of n-hexadecane in 88 parts of dichloromethane, slowly drop the oil phase solution into 660 parts of 0.8% aqueous solution of sodium dodecylsulfonate, in the emulsifier at 2800r / Stir at min speed for 30 minutes, then reduce the speed to 500r / min, heat the emulsion until the temperature reaches 35-40 degrees Celsius, continue stirring for 2 hours, filter, wash, and dry to obtain the polysulfone capsule wall—n-hexadecane capsule core The phase change microcapsules have a phase change temperature of 18.6 degrees Celsius and a phase change latent heat of 98 kJ / kg as tested by DSC, and an average particle size of 45 microns tested by a laser particle size analyzer.
[0095] Step 2: Prepare expanded perlite shaped phase change particles with a phase change temperature of 26-28 degrees Celsius
[0096] Mix 10 parts of expa...
Embodiment 3
[0100] Step 1: Prepare phase change microcapsules with a phase change temperature of 18-20 degrees Celsius
[0101] Dissolve 15 parts of polymethyl methacrylate and 20 parts of n-hexadecane in 140 parts of dichloromethane, slowly drop the oil phase solution into 1050 parts of 0.9% concentration of polyvinyl alcohol aqueous solution, in the emulsifier at 2800r / Stir at min speed for 30 minutes, then reduce the speed to 500r / min, heat the emulsion until the temperature reaches 35-40 degrees Celsius, continue stirring for 2 hours, filter, wash and dry to obtain the polymethyl methacrylate capsule wall—positive ten Hexane capsule core phase change microcapsules have a phase change temperature of 18.2 degrees Celsius and a latent heat of phase change of 105 kJ / kg tested by DSC, and an average particle size of 52 microns tested by a laser particle size analyzer.
[0102] Step 2: Prepare expanded perlite shaped phase change particles with a phase change temperature of 26-28 degrees C...
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