Large-area cadmium sulfide film preparing method
A thin-film preparation and cadmium sulfide technology, which is applied in the fields of final product manufacturing, sustainable manufacturing/processing, semiconductor/solid-state device manufacturing, etc., can solve the problems of environmental pollution of ammonia water, waste of resources, etc., achieve low reaction temperature, avoid corrosion, and improve performance good effect
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Embodiment 1
[0047] A large-area cadmium sulfide thin film is prepared by using a chemical water bath method based on a copper indium gallium selenide substrate. The preparation steps are as follows:
[0048] Preparation of CIGS substrate: Firstly, the CIGS absorbing layer prepared on the glass substrate must be obtained.
[0049] 1) Cleaning of soda lemon glass
[0050] ① Soak a 10cm×10cm soda glass in heavy potassium hydroxide solution (a solution made of 300 grams of potassium hydroxide and 3 liters of deionized water) for 2 hours; ② Put the rinsed soda glass in a concentration of 99.5 % acetone solution, put it into an ultrasonic cleaning machine for cleaning with an ultrasonic frequency of 50kHz and a time of 30min, which can be properly heated to 40°C; ③ Take the soda glass out of the acetone solution and rinse it with deionized water; ④ Clean the washed Soda-lemon glass substrates were cleaned with alcohol and dried with nitrogen.
[0051] 2) Preparation of molybdenum back contact...
Embodiment 2
[0064] A large-area cadmium sulfide thin film is prepared by using a chemical water bath method based on a copper indium gallium selenide substrate. The preparation steps are as follows:
[0065] Preparation of CIGS substrate: Firstly, the CIGS absorbing layer prepared on the glass substrate must be obtained.
[0066] 1) Cleaning of soda lemon glass
[0067] ① Soak a 10cm×10cm soda glass in heavy potassium hydroxide solution (a solution made of 300 grams of potassium hydroxide and 3 liters of deionized water) for 2 hours; ② Put the rinsed soda glass in a concentration of 99.5 % acetone solution, put it into an ultrasonic cleaning machine for cleaning with an ultrasonic frequency of 50kHz and a time of 30min, which can be properly heated to 40°C; ③ Take the soda glass out of the acetone solution and rinse it with deionized water; ④ Clean the washed Soda-lemon glass substrates were cleaned with alcohol and dried with nitrogen.
[0068] 2) Preparation of molybdenum back contact...
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