Novel red light conversion film and preparation method and application thereof
A technology of light conversion film and red phosphor, which is applied in the field of agricultural light conversion, can solve problems such as environmental threats and no light conversion effect, and achieve the effects of avoiding environmental problems, abundant reserves, and excellent optical performance
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Embodiment 1
[0048] The preparation method of the new red light conversion film can be divided into three stages: cellulose dissolution, compounding process, and curing into film:
[0049] Pre-cool 100 g of a combined aqueous solution containing 7wt% NaOH / 12wt% urea to -12°C~-13°C, add a certain amount of cotton paddle (purchased from Hubei Chemical Fiber Group Co., Ltd., DP=580), and stir quickly to obtain 4wt % Cellulose solution. Then take 0.10g of Sr 2 Si 5 N 8 :Eu 2+ (Light conversion agent Sr 2 Si 5 N 8 :Eu 2+ Excitation and emission spectra, see figure 1 ;Light conversion agent Sr 2 Si 5 N 8 :Eu 2+ SEM, see figure 2 ) Was added to the above solution, continued to stir for 30 minutes to make it uniformly dispersed, and the bubbles were removed by a high-speed centrifuge to obtain a composite solution (the mass ratio of the light conversion agent to the cellulose in the composite solution was 1:40). After casting the composite solution on the glass plate to form a film, immediately imme...
Embodiment 2
[0051] 100g of 50wt% N-methylmorpholine-N-oxide aqueous solution was distilled under reduced pressure at 85°C until the water content dropped to about 13.3wt%, then 3g cotton pulp was added and stirred for a period of time to obtain a transparent , Light brown cellulose / NMMO solution (where the final concentration of cellulose is 5.2 wt%). Then add 0.2g of Sr 2 Si 5 N 8 :Eu 2+ , Continue to stir for 30 minutes to make it uniformly dispersed in the cellulose mixed solution, remove bubbles, and obtain a composite solution (the mass ratio of the light conversion agent to the cellulose in the composite solution is 1:15). After the composite solution is cast on a hot glass plate to form a film, it is cured and formed, washed with distilled water, and then laid flat on the glass plate to dry naturally to obtain a new red light-converting film.
Embodiment 3
[0053] 100 g of a combined aqueous solution containing 7 wt% NaOH / 12 wt% urea is pre-cooled to -12°C to -13°C, a certain amount of cotton paddle is added, and the mixture is stirred rapidly to obtain a 4 wt% cellulose solution. Then add 0.20g of CaAl 12 O 19 :Mn 4+ , Continue to stir for 30 minutes to make it uniformly dispersed in the cellulose solution, and remove the bubbles by a high-speed centrifuge to obtain a composite solution (the mass ratio of the light conversion agent to the cellulose in the composite solution is 1:20). After casting the composite solution on the glass plate to form a film, immediately immerse it into 5wt% H 2 SO 4 It is solidified in the solution and formed, after 2 minutes, it is taken out and washed, and it is laid flat on a glass plate and dried naturally to obtain a new type of red light conversion film. The excitation and emission spectra of the obtained light conversion film are as follows image 3 Shown (measured with a fluorescence spectrome...
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