Paper tube glue and preparation method therefor
A glue and paper tube technology, applied in the direction of adhesives, non-polymer adhesive additives, adhesive additives, etc., can solve the problem of poor compressive strength and creep resistance of paper tubes, decreased compressive strength of paper tubes, and adhesive strength. Low and other problems, to achieve the effect of short initial adhesion time, no warpage of bonding, and good initial adhesion
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Embodiment 1
[0019] A paper tube glue, made of the following raw materials in parts by weight: 15 parts of ethyl α-cyanoacrylate, 7 parts of coumarone-indene resin, 2 parts of dibutyl phthalate, 5 parts of calcium carbonate, talc 3 parts of powder, 10 parts of 6-di-tert-butyl-p-cresol, 5 parts of N-phenyl-β-naphthylamine, and 25 parts of water.
[0020] The preparation method of above-mentioned paper tube glue comprises the following steps:
[0021] 1) Put water into the mixing equipment according to the weight part, heat to 40°C, add ethyl α-cyanoacrylate, coumarone-indene resin and dibutyl phthalate, stir and mix, then adjust the pH with acetic acid to 6.5, then stirred at a speed of 200r / min for 45min to make a mixed solution A for later use;
[0022] 2) Put the calcium carbonate into the pulverizing equipment, pulverize to 300 mesh, make powder B, and set aside;
[0023] 3) Put the talcum powder into the jet milling equipment, pulverize to 500 mesh, make powder C, set aside;
[0024...
Embodiment 2
[0028] A paper tube glue, made of the following raw materials in parts by weight: 35 parts of ethyl α-cyanoacrylate, 3 parts of coumarone-indene resin, 8 parts of dibutyl phthalate, 1 part of calcium carbonate, talc 6 parts of powder, 10 parts of 6-di-tert-butyl-p-cresol, 8 parts of N-phenyl-β-naphthylamine, and 20 parts of water.
[0029] The preparation method of above-mentioned paper tube glue comprises the following steps:
[0030] 1) Put water into the stirring equipment according to the weight part, heat to 50°C, add ethyl α-cyanoacrylate, coumarone-indene resin, dibutyl phthalate, stir and mix, and then adjust the pH with acetic acid to 5.5, then stirred at a speed of 350r / min for 30min to make a mixed solution A for later use;
[0031] 2) Calcium carbonate is put into the pulverizing equipment, pulverized to 400 mesh, made into powder B, and set aside;
[0032] 3) Put the talcum powder into the jet milling equipment, pulverize to 600 mesh, make powder C, set aside; ...
Embodiment 3
[0037] A paper tube glue, made of the following raw materials in parts by weight: 30 parts of ethyl α-cyanoacrylate, 5 parts of coumarone-indene resin, 5 parts of dibutyl phthalate, 4 parts of calcium carbonate, talc 5 parts of powder, 12 parts of 6-di-tert-butyl-p-cresol, 4 parts of N-phenyl-β-naphthylamine, and 35 parts of water.
[0038] The preparation method of above-mentioned paper tube glue comprises the following steps:
[0039] 1) Put water into the mixing equipment according to the weight part, heat to 45°C, add ethyl α-cyanoacrylate, coumarone-indene resin and dibutyl phthalate, stir and mix, and then adjust the pH with acetic acid to 6.0, then stirred at a speed of 300r / min for 40min to make a mixed solution A for later use;
[0040] 2) Calcium carbonate is put into the pulverizing equipment, pulverized to 350 mesh, made into powder B, and set aside;
[0041] 3) Put the talc powder into the jet milling equipment, and pulverize it to 550 mesh, and make powder C, a...
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