Fully synthetic cutting fluid composition
A technology of composition and cutting fluid, which is applied in lubricating compositions, additives, petroleum industry, etc., and can solve problems such as floating or accumulation, increased consumption of concentrated liquid, and poor sanitation on site
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Embodiment 1
[0083] The preparation of embodiment 1 polyisobutylene o-cresol
[0084] In a 500ml four-necked flask equipped with a stirrer, thermometer, condenser and dropping funnel, add 34.93g o-cresol, 6.88g catalyst boron trifluoride ether, 100ml n-hexane solvent and 161.61 polyisobutylene (Mn=1000) g was reacted at 80°C for 2h. After the reaction, use 5% potassium hydroxide solution to wash the reaction mixture once, and wash it with hot water to neutrality to remove the catalyst, then distill off the solvent and unreacted o-cresol under reduced pressure. The synthetic product is polyisobutylene o-cresol, and its hydroxyl value is 53.49 mg / g. The hydroxyl value determination method is the acetic anhydride method in GB / T7383-2007.
Embodiment 2
[0094] Add 45.66g of DB-1 detergent and dispersant prepared in Comparative Example 1 into a stirred 250ml reaction kettle, add 0.96g of hexamethylene diisocyanate (HDI), stir, and heat up to 90 °C, react at this temperature for 3.5 hours, stop heating, continue to pass nitrogen until the reactant cools to room temperature, collect the product, and obtain the Mannich base urea derivative dispersant MN-1 of the present invention.
Embodiment 3
[0096] Add 44.12g of the DB-2 detergent and dispersant prepared in Comparative Example 2 into a stirred 250ml reaction kettle, add 4.71g of hexamethylene diisocyanate (HDI), stir, and heat up to 100 °C, react at this temperature for 4 hours, stop heating, continue to pass nitrogen until the reactant is cooled to room temperature, collect the product, and obtain the Mannich base urea derivative dispersant MN-2 of the present invention.
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Abstract
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