One-step fluorescent quantitative RT-PCR detection primers and kits for Nodamura virus in Macrobrachium rosenbergii
A Noda Village virus and fluorescence quantitative technology, which is applied in the determination/testing of microorganisms, microorganisms, and methods based on microorganisms, etc., can solve the problems of low sensitivity, inability to quantify, and easy cross-contamination, and achieve sensitive and rapid operation, rapid detection, The effect of convenient operation
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Embodiment 1
[0032] Embodiment 1, primer design and synthesis
[0033] A pair of specific primers were designed according to the conserved region of the MrNV gene sequence (GenBank No. HQ287005). The size of the augmented fragment is 119bp, which was synthesized by Treasure Bioengineering (Dalian) Co., Ltd., diluted with DEPC-treated water to 20 pmol / μl, and stored at -20°C for later use.
Embodiment 2
[0034]Embodiment 2, the establishment of one-step fluorescent quantitative RT-PCR detection method
[0035] (1) Sample preparation
[0036] Take 50-100 mg of the gill filaments and muscle tissue of the juvenile or adult shrimp to be tested, add 500 μl of TN buffer (20 mM Tris / HCl, 0.4 M NaCl, pH 7.4) to homogenate, and centrifuge to obtain the supernatant. The RNA extraction kit (QIAamp Viral RNA MiniKit) was used to extract the total RNA of Macrobrachium rosenbergii Nodamura virus according to its instructions, and the purity and concentration of virus RNA were measured with a nucleic acid protein analyzer, and stored at -80°C for later use.
[0037] (2) Preparation of standard products
[0038] The MrNV capsid protein gene fragment was amplified using the previously constructed and preserved plasmid as a template, and cloned into the pGM-T vector. After the positive identification, the plasmid DNA was extracted and linearized by single enzyme digestion, and the recovered pr...
Embodiment 3
[0047] Embodiment 3, the assembly of detection kit
[0048] According to the research results of Examples 1 and 2, a detection kit was assembled for easy use. The kit contains the following reagents:
[0049] (1) One-step fluorescence quantitative RT-PCR reaction solution (solution A): a total of 2.3mL, each dose of reaction solution is 23μL, composed of 2×OneStep RT-PCR Buffer 12.5 μL, PrimeScript 1 step Enzyme Mix 1.0 μL, upstream and downstream primers with a concentration of 10 μmol / L 1.0 μL each, ROX Reference Dye II (50X) 0.5 μL, H 2 O 7.0 μL composition.
[0050] (2) Positive control (solution P): RNA fragment containing MrNV gene, 200 μL;
[0051] (3) Negative control (N solution): RNA fragments without MrNV gene, 200 μL;
[0052] (4) Working standard: including 1×10 8 (B1 liquid), 1×10 7 (B2 liquid), 1×10 6 (B3 solution), 1×10 5 (B4 liquid), 1×10 4 (B5 liquid), 1×10 3 (B6 liquid), 1×10 2 (B7 liquid), 1×10 1 (B8 solution) 200 μL each copy / μL standard RNA. ...
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