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Sulfur-free and efficient cleaning method for sugar juice

A high-efficiency technology for sugar juice, applied in the purification of sugar juice, the use of physical methods to purify, and sucrose production. It can solve the problems of increasing sugar loss and production energy consumption, high material quality requirements, and more sucrose conversion. The effect of high chemical depth development value, less sugar loss and simple treatment process

Active Publication Date: 2018-08-17
广东省科学院生物与医学工程研究所
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0009] Chinese Patent (Application No.) 201410088309.0 discloses a sulfur-free clarification method for sugar cane sugar production. The lime method is used for primary precipitation clarification and tannin and calcium bicarbonate reaction for secondary precipitation purification to obtain sulfur-free clear sugar juice. Two steps The temperature of the clarification process is in the boiling state of the sugar juice, and the sedimentation process is carried out by the difference in solid-liquid specific gravity in the solution, which is greatly affected by the structure of the sedimentation tank, fluid flow state, particle size, temperature and other factors. The time is 30-45min, the settling time of the multi-layer settler is 60-75min, the two-stage settling process, the total residence time of the sugar juice in the settler is longer (the total residence time is 60-150min), the sucrose content is converted more, and the mud juice in this method is returned to the mixed juice tank, which further increases the sugar loss and production energy consumption
The more advanced cleaning methods of sugar liquid include membrane separation method and ion exchange method. Membrane separation method has many problems of membrane material and membrane attenuation, so far it has not been applied in sugar factories with low product added value. There are many applications and promotions in factories, and advanced ion exchange equipment has also been introduced in China, but there are problems such as high material quality requirements and complicated operations, and domestic sugar refineries have not been able to promote them.

Method used

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  • Sulfur-free and efficient cleaning method for sugar juice
  • Sulfur-free and efficient cleaning method for sugar juice

Examples

Experimental program
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Effect test

Embodiment 1

[0035]A sulfur-free and efficient cleaning method for sugar juice, the specific steps are as follows:

[0036] (1) Pre-treatment of the sugar juice once floating: add lime milk and phosphoric acid to the sugar juice, adjust the total phosphoric acid value in the sugar juice to 200ppm, control the pH value of the sugar juice at 7.5, control the primary heating temperature at 60°C, and then enter the bubble making process - Flocculation reactor, add flocculant 4ppm after foaming sugar juice, fully react;

[0037] (2) One-time flotation clarification of sugar juice: the sugar juice treated before the first flotation flows into the first-time flotation clarifier for solid-liquid separation, and the scum on the upper layer of the clarifier is collected into the scum storage tank through the scum removal system, and the sugar juice is cleared once It is discharged through the clear juice discharge pipe in the lower layer of the clarifier and collected into the primary floating clear...

Embodiment 2

[0042] A sulfur-free and efficient cleaning method for sugar juice, the specific steps are as follows:

[0043] (1) Pre-treatment of the sugar juice once floating: add lime milk and phosphoric acid to the sugar juice, adjust the total phosphoric acid value in the sugar juice to 300ppm, control the pH value of the sugar juice at 8.0, control the primary heating temperature at 65°C, and then add 100ppm of composite clarifying agent (chitosan quaternary ammonium salt and polyaluminum chloride with a mass ratio of 2:1) enters the bubble-flocculation reactor, and adds 4ppm of flocculant after the sugar juice is bubbled to fully react;

[0044] (2) One-time flotation clarification of sugar juice: the sugar juice treated before the first flotation flows into the first-time flotation clarifier for solid-liquid separation, and the scum on the upper layer of the clarifier is collected into the scum storage tank through the scum removal system, and the sugar juice is cleared once It is d...

Embodiment 3

[0049] A sulfur-free and efficient cleaning method for sugar juice, the specific steps are as follows:

[0050] (1) Pre-treatment of the sugar juice once floating: add lime milk and phosphoric acid to the sugar juice, adjust the total phosphoric acid value in the sugar juice at 250ppm, control the pH value of the sugar juice at 8.5, control the primary heating temperature at 70°C, and then add 150ppm of composite clarifying agent (chitosan quaternary ammonium salt and polyaluminum chloride with a mass ratio of 2:1) enters the bubble-flocculation reactor, and adds 4ppm of flocculant after the sugar juice is bubbled to fully react;

[0051] (2) One-time flotation clarification of sugar juice: the sugar juice treated before the first flotation flows into the first-time flotation clarifier for solid-liquid separation, and the scum on the upper layer of the clarifier is collected into the scum storage tank through the scum removal system, and the sugar juice is cleared once It is d...

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Abstract

The invention belongs to the technical field of sugar industries and discloses a sugar juice sulfur-free efficient cleaning method. After preliming, heating, foaming and flocculant adding are conducted on sugar juice, one-time floating clarification is conducted, large-particle non-sugar components in the sugar juice are removed; after secondary preliming, heating, foaming and flocculant adding are conducted on the one-time floating clarification sugar juice, secondary floating clarification is conducted; the sulfur-free cleaning process of the sugar juice is completed on the sugar juice obtained through secondary floating clarification through a sugar juice filtering and separating system. According to the sugar juice sulfur-free efficient cleaning method, the cleaning method of two levels of floating of the sugar juice is mainly adopted, and clean and complete sufur-free and carbonic-acid-free processing is achieved on the sugar juice, the equipment technology is simple, automatic continuous production is convenient, and the production efficiency is obviously improved. The obtained clean sugar juice is high in quality and is superior to clean sugar juice obtained through a traditional sulfurous method, and a very good application prospect is achieved.

Description

technical field [0001] The invention belongs to the technical field of sugar industry, and in particular relates to a sulfur-free and efficient cleaning method for sugar juice. Background technique [0002] At present, the sugar industry adopts two processes to produce cultivated white sugar, that is, the carbonation method and the sulfurous acid method cleaning technology. Carbonation sugar production process: Due to the production of a large amount of alkaline (8.0<pH<11) solid waste-filter mud (the ratio of wet filter mud to raw materials is about 5-10%), it is difficult to handle and the discharge is large, causing environmental damage pollution, which limits its application. Sulfurous acid sugar production process: due to the unstable reductive bleaching effect of sulfurous acid on pigments, the sugar will return to color after long storage, the content of ash and insoluble impurities is high, and the sulfur content of the product is above 20mg / kg (the national s...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C13B20/00C13B20/02C13B20/16
CPCC13B20/00C13B20/02C13B20/16
Inventor 黄向阳许广球高俊永张平军孙潇莫柳珍谢武装黄廷冠梁波陆金杨欢符瑞华陆浩湉谢晋谋
Owner 广东省科学院生物与医学工程研究所
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