Low-loss soft magnetic ferrite material and preparation method thereof
A technology of soft ferrite and low loss, which is applied in the field of low loss soft ferrite material and its preparation, can solve the problem of unsatisfactory magnetic core loss, etc., and achieve high magnetic permeability, high resistivity, and high magnetic permeability Effect
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[0027] Reference figure 1 , The preparation method of a low-loss soft ferrite material proposed by the present invention includes the following steps:
[0028] S1. After adding the adsorbent and emulsifier into the water and stirring uniformly, the first material is obtained after 25-40 minutes of ultrasonic dispersion;
[0029] S2. Add ferric nitrate, manganese nitrate, zinc nitrate and nickel nitrate into water to dissolve to obtain the second material;
[0030] S3. Add the second material dropwise to the first material, then evaporate and dry, then roast, and cool to obtain a powder material;
[0031] S4. Add neodymium oxide, vanadium oxide, niobium oxide, boron oxide, calcium carbonate, lithium carbonate, barium carbonate, silicon dioxide and adhesives to the powder material for spray granulation, tableting, and sintering to obtain low-loss soft Ferrite material.
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[0033] Example 1
[0034] The present invention proposes a low-loss soft ferrite material. Its raw materials include main materials and auxiliary materials. The main materials include 57 parts of iron nitrate, 42 parts of manganese nitrate, 9 parts of zinc nitrate, and 10 parts of nickel nitrate. Based on the total weight of the main materials, the auxiliary materials include: neodymium oxide 300ppm, vanadium oxide 400ppm, niobium oxide 400ppm, boron oxide 700ppm, calcium carbonate 50ppm, lithium carbonate 100ppm, barium carbonate 20ppm, silicon dioxide 800ppm, adhesive 2000ppm, Adsorbent 5×10 6 ppm, 300 ppm emulsifier.
[0035] The method for preparing the above-mentioned low-loss soft ferrite material provided by the present invention includes the following steps:
[0036] S1. After adding the adsorbent and emulsifier into the water, stir uniformly, and ultrasonically disperse for 25 minutes to obtain the first material;
[0037] S2. Add ferric nitrate, manganese nitrate, zinc nitr...
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[0040] Example 2
[0041] The present invention proposes a low-loss soft ferrite material. Its raw materials include main materials and auxiliary materials. The main materials include 58 parts of iron nitrate, 41 parts of manganese nitrate, 10 parts of zinc nitrate, and 9.4 parts of nickel nitrate. Based on the total weight of the main materials, the auxiliary materials include: 320ppm neodymium oxide, 360ppm vanadium oxide, 450ppm niobium oxide, 600ppm boron oxide, 100ppm calcium carbonate, 90ppm lithium carbonate, 50ppm barium carbonate, 600ppm silica, 2200ppm adhesive, Adsorbent 4×10 6 ppm, 350 ppm emulsifier.
[0042] The method for preparing the above-mentioned low-loss soft ferrite material provided by the present invention includes the following steps:
[0043] S1. After adding the adsorbent and emulsifier into the water and stirring uniformly, the first material is obtained after 40 minutes of ultrasonic dispersion, wherein the weight ratio of the adsorbent and water is 2:6;...
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