Novel nano-carbon-fiber heating floor and preparation method thereof
A nano-carbon fiber and flooring technology, applied in heating methods, lighting and heating equipment, electric heating systems, etc., to achieve uniform resistance distribution, improve usability, and uniform distribution
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Embodiment 1
[0028] (1) Place the nano-polyacrylonitrile fiber prepared by electrospinning in an oven, use air as the medium, heat up to 240°C at a rate of 2°C / min for heat treatment for 90 minutes, and then carbonize at 800°C for 50 minutes under a nitrogen atmosphere. A carbonized nano-polyacrylonitrile fiber with a diameter of 10 nm and an aspect ratio of 200 was obtained.
[0029] (2) In parts by weight, 35 parts of plant protoplasmic fibers and 5 parts of quaternary ammonium salt cationic surfactants are stirred until uniform under closed and normal temperature conditions, and 15 parts of carbonized processed Polyacrylonitrile nano-carbon fiber and nano-graphite powder, the amount of nano-graphite powder is 0.1 parts by volume of carbonized polyacrylonitrile nano-carbon fiber, stirred at a high speed of 1200rpm / min, and made into a sheet-shaped flexible polymer material by hot pressing process .
[0030] (3) The two ends of the sheet-shaped flexible polymer material prepared in step ...
Embodiment 2
[0033] (1) Place the nano-polyacrylonitrile fiber prepared by electrospinning in an oven, use air as the medium, heat-treat at 250°C at a rate of 5°C / min for 120min, and then carbonize at 1000°C for 60min under a nitrogen atmosphere. A carbonized nano-polyacrylonitrile fiber with a diameter of 150 nm and an aspect ratio of 400 was obtained.
[0034] (2) In parts by weight, 60 parts of plant protoplasmic fibers and 12 parts of quaternary ammonium salt cationic surfactants are stirred until uniform under closed and normal temperature conditions, and 35 parts of carbonized processed Polyacrylonitrile nano-carbon fiber and nano-graphite powder, the amount of nano-graphite powder is 0.2 parts by volume of carbonized polyacrylonitrile nano-carbon fiber, stirred at a high speed of 2000rpm / min, and made into sheet-shaped flexible polymer material by hot pressing process .
[0035] (3) The two ends of the sheet-shaped flexible polymer material prepared in step (2) were fixed with silv...
Embodiment 3
[0038](1) Place the nano-polyacrylonitrile fiber prepared by electrospinning in an oven, use air as the medium, heat-treat at 245°C at a rate of 3°C / min for 100min, and then carbonize at 900°C for 55min under a nitrogen atmosphere. A carbonized nano-polyacrylonitrile fiber with a diameter of 50 nm and an aspect ratio of 300 was obtained.
[0039] (2) In parts by weight, 40 parts of plant protoplasm fibers and 8 parts of quaternary ammonium salt cationic surfactants are stirred until uniform under closed and normal temperature conditions, and 20 parts of carbonized processed Polyacrylonitrile nano-carbon fiber and nano-graphite powder, the amount of nano-graphite powder is 0.15 parts by volume of carbonized polyacrylonitrile nano-carbon fiber, stirred at a high speed of 1500rpm / min, and made into sheet-shaped flexible polymer material by hot pressing process .
[0040] (3) The two ends of the sheet-shaped flexible polymer material prepared in step (2) were fixed with silver so...
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