Dynamic gradient embedding method for purple corn cob anthocyanin

A technology of anthocyanins and purple corn, applied in chemical instruments and methods, pharmaceutical formulations, food science, etc., can solve the effects of unexamined anthocyanin embedding efficiency, embedding yield anthocyanin stability, and undisclosed anthocyanin Gradient embedding method, no purple corn cob embedding and other problems, to achieve the effect of improving embedding efficiency, yield and storage stability, improving storage stability, and improving film-forming effect

Active Publication Date: 2016-01-13
JIANGSU FOOD & PHARMA SCI COLLEGE
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0007] As a class of functional substances, anthocyanins have poor stability and are sensitive to factors such as light, heat and pH, which limits their application in industry. Therefore, the research on the stability of anthocyanins has become a research hotspot in the field of anthocyanins.
As disclosed in some of the above-mentioned patent documents, the method of using co-coloring agents or embedding is currently a common method for improving the stability of anthocyanins. Among them, the embedding method is the most common, but none of the above-mentioned patent documents examines the use of gradient concentrations for multiple embedding. The impact on anthocyanin embedding efficiency, embedding yield, and anthocyanin stability has not been disclosed. The anthocyanin gradient embedding method is not disclosed; in addition, the commonly used high concentration of gum arabic increases the cost of raw materials significantly; moreover, spray drying It is necessary to control the concentration of the feed liquid or add an anti-caking agent to avoid the problem of caking, and the process is complicated
[0008] In terms of anthocyanin embedding technology, at present, most of the patent documents published in China focus on blackberry, blueberry, purple sweet potato, etc., and there is no patent document on purple corncob embedding

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0019] (1) Preparation of wall materials Use distilled water to prepare colloidal wall material solutions with concentrations of 100g / L, 140g / L, and 180g / L respectively. Among them, every liter of 100g / L wall material colloid wall material solution contains 20g octenyl succinic anhydride modified gum arabic, 40g maltodextrin, 40g hydroxypropyl β-cyclodextrin, 0.05g EDTA-2Na; 140g / L per liter The wall material colloid wall material solution contains 20g octenyl succinic anhydride modified gum arabic, 60g maltodextrin, 60g hydroxypropyl β-cyclodextrin, 0.05g EDTA-2Na; every liter of 180g / L wall material colloid wall material solution contains 20g octenyl succinic anhydride modified gum arabic, 80g maltodextrin, 80g hydroxypropyl β-cyclodextrin, 0.05g EDTA-2Na;

[0020] ⑵The preparation of the core material uses 80% ethanol solution containing 1% citric acid as the extractant, the ratio of purple corncob powder to the extractant is 1:8 (W / V), and extracts twice at 55°C, each extr...

Embodiment 2

[0024] (1) Preparation of wall materials Use distilled water to prepare colloidal wall material solutions with concentrations of 110g / L, 150g / L, and 190g / L respectively. Among them, every liter of 110g / L wall material colloid wall material solution contains 25g octenyl succinic anhydride modified gum arabic, 45g maltodextrin, 40g hydroxypropyl β-cyclodextrin, 0.10g EDTA-2Na; 150g / L per liter The wall material colloid wall material solution contains 25g octenyl succinic anhydride modified gum arabic, 65g maltodextrin, 60g hydroxypropyl β-cyclodextrin, 0.10g EDTA-2Na; every liter of 190g / L wall material colloid wall material solution contains 25g octenyl succinic anhydride modified gum arabic, 85g maltodextrin, 80g hydroxypropyl β-cyclodextrin, 0.10g EDTA-2Na;

[0025] ⑵The preparation of the core material uses 80% ethanol solution containing 1% citric acid as the extractant, the ratio of purple corncob powder to the extractant is 1:8 (W / V), and extracts twice at 55°C, each extr...

Embodiment 3

[0029] (1) Preparation of wall materials Use distilled water to prepare colloidal wall material solutions with concentrations of 120g / L, 160g / L, and 200g / L respectively. Among them, every liter of 120g / L wall material colloid wall material solution contains 30g octenyl succinic anhydride modified gum arabic, 45g maltodextrin, 45g hydroxypropyl β-cyclodextrin, 0.10g EDTA-2Na; 160g / L per liter Wall material colloid wall material solution contains 30g octenyl succinic anhydride modified gum arabic, 65g maltodextrin, 65g hydroxypropyl β-cyclodextrin, 0.10g EDTA-2Na; every liter of 200g / L wall material colloid wall material solution contains 30g octenyl succinic anhydride modified gum arabic, 85g maltodextrin, 85g hydroxypropyl β-cyclodextrin, 0.10g EDTA-2Na;

[0030] ⑵The preparation of the core material uses 80% ethanol solution containing 1% citric acid as the extractant, the ratio of purple corncob powder to the extractant is 1:9 (W / V), and extracts twice at 55°C, each extracti...

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Abstract

The present invention provides a dynamic gradient embedding method for purple corn cob anthocyanin. The embedding method takes octenyl succinic anhydride modified acacia, dextrin and hydroxypropyl beta-cyclodextrin as a wall material, and takes macropore resin purified purple corn cob anthocyanin through a water extraction method as a cob material. In order to improve the embedding efficiency, the embedding yield and the storage stability of the anthocyanin, the method provided by the present invention adopts a dynamic gradient embedding method to control wall material concentrations from low to high, thus achieving embedding of the anthocyanin for many times. Through measurement, the embedding efficiency of the purple corn cob anthocyanin microcapsules reaches 94-99%, and the embedding yield of the same reaches 92-96%. Compared to an embedding method with an equal concentration in the whole course, the embedding efficiency is improved by 20-35%, and the embedding yield is improved by 25-40%. After 60-70 hours at room temperature in daylight, the preservation rate of the gradient embedded purple corn cob anthocyanin can reach 90% or above, and the light stable time of the same is shortened by 500-600% compared with equal concentration embedding method in the whole course.

Description

technical field [0001] The invention relates to the technical field of deep processing of grains, in particular to a method for embedding purple corncob anthocyanins, in particular to a dynamic gradient embedding method to improve the embedding efficiency, embedding yield and storage of purple corncob anthocyanins stability. Background technique [0002] Anthocyanins are widely distributed, and it is known that there are more than 600 kinds of anthocyanins in nature. Anthocyanins have a higher antioxidant capacity than common antioxidants such as vitamin C and vitamin E, and have strong abilities to scavenge free radicals, antibacterial, anti-inflammatory and inhibit the growth of cancer cells. Anthocyanins can also be used as natural food additives for cooling Coloring of foods such as beverages, jellies, and candies. Therefore, it has attracted widespread attention from scholars in the fields of food, cosmetics, nutrition and pharmacy. [0003] At present, the researche...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09B67/02C09B67/08C09B61/00A23L5/40A23L33/10A61K9/48A61K31/7048A61K47/40A61K8/60A61K8/11A61Q19/08A61Q17/04A61P39/06A61P35/00A61P31/04A61P29/00
Inventor 焦宇知翟玮玮王德兵
Owner JIANGSU FOOD & PHARMA SCI COLLEGE
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