Unlock instant, AI-driven research and patent intelligence for your innovation.

Biodegradable organic baseplate material and preparation method thereof

An organic substrate, biological technology, applied in metal material coating process, ion implantation plating, coating and other directions, can solve problems such as pollution, achieve the effects of strong operability, low thermal expansion coefficient, and simple preparation method

Active Publication Date: 2016-04-20
SHENZHEN INST OF ADVANCED TECH CHINESE ACAD OF SCI
View PDF4 Cites 4 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] In view of this, the purpose of the present invention is to overcome the shortcomings and deficiencies of the prior art. On the one hand, the present invention provides a method for preparing a biodegradable organic substrate material, which uses biodegradable nanocellulose as a raw material , carbon nanotubes are used as dielectrically enhanced particles, the preparation process is environmentally friendly, the solvent used is aqueous solution, no organic solvent is involved, the preparation method is simple and operable, and it can be scaled up for production, which solves the environmental pollution of current organic substrate materials

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Biodegradable organic baseplate material and preparation method thereof
  • Biodegradable organic baseplate material and preparation method thereof
  • Biodegradable organic baseplate material and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0030] According to the mass ratio of 1:20, carbon nanotubes with a diameter of 5nm and a length of 5 μm are mixed with a mass fraction of 2.5% nanocellulose aqueous solution, wherein the nanocellulose has a diameter of 20nm and a length of 10μm. The power is 1000W, the time is 24h, and the nanocellulose-carbon nanotube mixed solution is obtained; the nanocellulose-carbon nanotube mixed solution is prepared by rod coating, and the nanocellulose-carbon nanotube film is prepared at a vacuum degree of -0.090MPa, drying at 80° C. for 4 hours to obtain a biodegradable composite material, and the mass fraction of carbon nanotubes in the biodegradable composite material is 0.5%. The upper and lower surfaces of the prepared biodegradable composite material were plated with copper by magnetron sputtering. The sputtering voltage was 160V, the sputtering time was 30min, and the sputtering temperature was 25°C. Finally, a biodegradable organic substrate material was obtained. Schematic di...

Embodiment 2

[0032] According to the mass ratio of 1:100, carbon nanotubes with a diameter of 40nm and a length of 500nm and a mass fraction of 0.5% nanocellulose aqueous solution are ultrasonically mixed evenly, wherein the diameter of the nanocellulose is 5nm and the length is 1 μm; The power is 100W, and the time is 12h, and the nanocellulose-carbon nanotube mixed solution is obtained; the nanocellulose-carbon nanotube mixed solution is prepared by vacuum filtration, and the nanocellulose-carbon nanotube film is prepared at a vacuum degree of - 0.090MPa, drying at 80°C for 4 hours to obtain a biodegradable composite material, the mass fraction of carbon nanotubes in the biodegradable composite material is 5.0%; the biodegradable composite material prepared by magnetron sputtering The upper and lower surfaces of the material were copper-plated, the sputtering voltage was 160V, the sputtering time was 30min, and the sputtering temperature was 25°C, finally a biodegradable organic substrate...

Embodiment 3

[0034] According to the mass ratio of 1:50, carbon nanotubes with a diameter of 20 nm and a length of 2 μm are mixed with a mass fraction of 5% nanocellulose aqueous solution by ultrasonic mixing, wherein the diameter of the nanocellulose is 10 nm and the length is 5 μm; The power is 500W, the time is 18h, and the nanocellulose-carbon nanotube mixed solution is obtained; the nanocellulose-carbon nanotube mixed solution is prepared by papermaking, and the nanocellulose-carbon nanotube film is prepared at a vacuum degree of -0.090 MPa, dry at 80°C for 4h. A biodegradable composite material is obtained, and the mass fraction of carbon nanotubes in the biodegradable composite material is 2.0%. The upper and lower surfaces of the prepared biodegradable composite material were plated with copper by magnetron sputtering. The sputtering voltage was 160V, the sputtering time was 30min, and the sputtering temperature was 25°C. Finally, a biodegradable organic substrate material was obta...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

PropertyMeasurementUnit
Tensile strengthaaaaaaaaaa
Thermal expansion coefficientaaaaaaaaaa
Diameteraaaaaaaaaa
Login to View More

Abstract

The invention provides a biodegradable organic baseplate material and a preparation method thereof. The preparation method comprises the following steps: (1) uniformly mixing carbon nano tubes and a nano-crystalline cellulose water solution according to the mass ratio of 1: (20-100) by adopting ultrasonic waves so as to obtain a nano-crystalline cellulose-carbon nano tube mixed solution; (2) carrying out film forming and vacuum drying on the nano-crystalline cellulose-carbon nano tube mixed solution so as to prepare a biodegradable composite material; (3) carrying out double-surface copper plating on the biodegradable composite material in a magnetron sputtering manner so as to prepare the biodegradable organic baseplate material. By taking the biodegradable nano-crystalline cellulose as a raw material and the carbon nano tubes as dielectric reinforced particles, the preparation process is environmentally friendly, the used solvent is the water solution, an organic solvent is not involved, the preparation method is simple and high in operability, and large-scale enlarged production can be realized; the prepared biodegradable organic baseplate material is high in dielectric constant, excellent in tensile strength and low in coefficient of thermal expansion, and has a biodegradable capability.

Description

technical field [0001] The invention relates to the field of composite materials, in particular to a biodegradable organic substrate material and a preparation method thereof. Background technique [0002] Organic substrate materials are important components in electronic packaging systems. The function of the organic substrate material is to carry and fix electronic components, and use the circuit pattern formed on the surface or inside to connect the circuit, and at the same time, it has the functions of insulation, heat conduction isolation and protection of components. The early organic substrate was a miniaturized copper-clad laminate, that is, a polymer compound and glass fiber cloth were combined to form a dielectric material (dielectric layer). After copper cladding on both sides, it became an organic substrate material with a sandwich structure. The physical and chemical properties of organic substrate materials are mainly determined by the intermediate dielectric ...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
IPC IPC(8): C08L1/02C08K7/24C08J5/18H01L23/14C23C14/20C23C14/35
CPCC08K7/24C08J5/18C08J2301/02C08K2201/003C08K2201/004C08K2201/011C08L2201/06C08L2203/16C23C14/205C23C14/35H01L23/145C08L1/02
Inventor 孙蓉曾小亮么依民许建斌
Owner SHENZHEN INST OF ADVANCED TECH CHINESE ACAD OF SCI