Carbon fiber reinforced halogen-free flame retardant polypropylene composite material and preparation method thereof
A flame-retardant polypropylene and composite material technology, applied in the field of polymer materials, can solve the problems of fast flame propagation rate, health hazards, and large release rate, and achieve improved compatibility and adhesion, high heat resistance And the effect of corrosion resistance, good halogen-free flame retardancy
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Embodiment 1
[0025] The preparation method of a carbon fiber reinforced halogen-free flame-retardant polypropylene composite material is as follows:
[0026] 1) Carbon fiber surface oxidation treatment:
[0027] Mix 60kg of nitric acid, 30kg of sodium nitrate and 10kg of hydrogen peroxide, add distilled water to make a 50% solution, then heat to 60°C, soak the carbon fiber in its 40°C solution for 60min, take it out and rinse with distilled water at a temperature of 80°C After drying, the carbon fiber with surface oxidation treatment is obtained;
[0028] 2) Preparation of red phosphorus flame retardant masterbatch
[0029] Mix 15kg of polypropylene resin, 70kg of red phosphorus, 12kg of zinc borate and 3kg of light stabilizer in a high-speed mixer. After mixing, the components are added to a twin screw extruder for melt blending, extrusion granulation, and drying Prepare red phosphorus flame retardant masterbatch;
[0030] 3) Mixing of raw materials
[0031] Weigh 60kg of polypropylene, 10kg of re...
Embodiment 2
[0035] The preparation method of a carbon fiber reinforced halogen-free flame-retardant polypropylene composite material is as follows:
[0036] 1) Carbon fiber surface oxidation treatment:
[0037] Mix 60kg of nitric acid, 30kg of sodium nitrate and 10kg of hydrogen peroxide, add distilled water to make a 55% solution, then heat to 70℃, soak the carbon fiber in its 60℃ solution for 120min, take it out and rinse with distilled water at a temperature of 100℃ After drying, the carbon fiber with surface oxidation treatment is obtained;
[0038] 2) Preparation of red phosphorus flame retardant masterbatch
[0039] Mix 15kg of polypropylene resin, 70kg of red phosphorus, 12kg of zinc borate and 3kg of compatibilizer in a high-speed mixer. After mixing, the components are added to a twin screw extruder for melt blending, extrusion granulation, and drying. Prepare red phosphorus flame retardant masterbatch;
[0040] 3) Mixing of raw materials
[0041] Weigh 70kg of polypropylene, 15kg of red ...
Embodiment 3
[0045] The preparation method of a carbon fiber reinforced halogen-free flame-retardant polypropylene composite material is as follows:
[0046] 1) Carbon fiber surface oxidation treatment:
[0047] Mix 60kg of nitric acid, 30kg of sodium nitrate and 10kg of hydrogen peroxide, add distilled water to make a 55% solution, then heat to 80°C, soak the carbon fiber in its 80°C solution for 180min, take it out and rinse with distilled water, at a temperature of 120°C After drying, the carbon fiber with surface oxidation treatment is obtained;
[0048] 2) Preparation of red phosphorus flame retardant masterbatch
[0049] 15kg of polypropylene resin, 70kg of red phosphorus, 12kg of zinc borate and 3kg of lubricant are fully mixed in a high-speed mixer. After mixing, the components are added to a twin screw extruder for melt blending, extrusion granulation, and drying. Obtain red phosphorus flame retardant masterbatch;
[0050] 3) Mixing of raw materials
[0051] Weigh 70kg of polypropylene, 10...
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