Preparing technology for bronze-base diamond grinding wheel
A preparation process and a technology for grinding wheel pieces, which are used in manufacturing tools, metal processing equipment, grinding/polishing equipment, etc., can solve the problems of complex diamond grinding wheel abrasive process, high production cost, inconvenience in mass application, etc., and achieve low equipment cost. , good quality, beneficial to the effect of industrial production
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preparation example Construction
[0024] A kind of preparation technology of bronze-based diamond grinding wheel sheet, it comprises the following steps:
[0025] (1) Preparation of titanium dioxide sol; when preparing titanium dioxide sol, first dissolve butyl titanate in absolute ethanol under stirring, then add diethanolamine, after the solution is evenly mixed, add ethanol aqueous solution dropwise, continue stirring, and then Aging to obtain titanium dioxide sol; the ratio of butyl titanate, water, diethanolamine and ethanol in the titanium dioxide sol is 1:1:1:(25-28). The invention adopts butyl titanate as an organic precursor, takes ethanol as an organic solvent, and prepares titanium dioxide sol through alcoholysis, hydrolysis and polycondensation reactions.
[0026] (2) Clean the diamond particles; when cleaning the diamond particles, first soak the diamond particles in hydrochloric acid solution, then rinse with deionized water until the pH value of the rinse solution is 7, and dry them, then ultras...
Embodiment 1
[0033] First dissolve butyl titanate in absolute ethanol under stirring, then add diethanolamine, after the solution is uniformly mixed, then add ethanol aqueous solution dropwise, continue stirring, and then age at room temperature for 1 hour to obtain titanium dioxide sol, in which butyl titanate The ratio of ester, water, diethanolamine, and ethanol is 1:1:1:25; at the same time, the diamond particles are first soaked in hydrochloric acid solution, and then rinsed with deionized water until the pH value of the rinse solution is 7, and dried. Dry, then ultrasonically clean with acetone, then rinse with deionized water and dry, then soak the cleaned diamond particles in the above titanium dioxide sol, take them out after standing, and then dry them in an oven at 70°C for 6 minutes, then cool ; and repeat the above steps 3 times; then place it in the muffle furnace, raise the temperature of the muffle furnace to 90°C and keep it for 30 minutes, then raise the temperature to 600...
Embodiment 2
[0035]First dissolve butyl titanate in absolute ethanol under stirring, then add diethanolamine, after the solution is uniformly mixed, then add ethanol aqueous solution dropwise, continue stirring, and then age at room temperature for 1 hour to obtain titanium dioxide sol, in which butyl titanate The ratio of ester, water, diethanolamine, and ethanol is 1:1:1:26.5; at the same time, the diamond particles are first soaked in hydrochloric acid solution, and then rinsed with deionized water until the pH value of the rinse solution is 7, and dried. Dry, then ultrasonically clean with acetone, then rinse with deionized water and dry, then soak the cleaned diamond particles in the above titanium dioxide sol, take them out after standing, and then dry them in an oven at 80°C for 5 minutes, then cool ; and repeat the above steps 4 times; then put it in the muffle furnace, raise the temperature of the muffle furnace to 95°C and keep it warm for 25min, then raise the temperature to 700°...
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