Graphene composite material for photoconversion and energy storage and preparation method
A technology of composite materials and graphite materials, applied in the field of graphene composite materials and preparation, can solve problems such as uneven dispersion, high equipment requirements, and cost reduction, and achieve the effects of uniform particle size, low cost, and cost reduction.
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Embodiment 1
[0023] Put 500g flake graphite into 1000g concentration and be in the aniline chlorate electrolyte solution of 20 mg / L, let stand for 1 day, allow the cation in the electrolyte solution to infiltrate between described graphite material layers, form intercalated graphite, filter and separate and take out all Describe intercalation graphite, 250g intercalation graphite and 2.5g magnesium carbonate blending are put into continuous screw reaction extruder, obtain extruding solid product, adopt sieve hole to screen out particle diameter and be the graphene of 10~20nm and magnesium carbonate powder body. Next, under the protection of nitrogen gas, the graphene and magnesium carbonate powders were added to a continuous screw reaction extruder, the temperature of the continuous screw reaction extruder was set to 300°C, the extrusion pressure was 20 MPa, and aniline chloride The acid salt and magnesium carbonate are decomposed by heat, and the decomposed carbon dioxide and ammonia gas ...
Embodiment 2
[0025] Put 500g flake graphite into 1000g concentration and be in the aniline chlorate electrolyte solution of 20 mg / L, let stand for 1 day, allow the cation in the electrolyte solution to infiltrate between described graphite material layers, form intercalated graphite, filter and separate and take out all Describe intercalation graphite, 250g intercalation graphite and 2.5g magnesium carbonate blending are put into continuous screw reaction extruder, obtain extruding solid product, adopt sieve hole to screen out particle diameter and be the graphene of 10~20nm and magnesium carbonate powder body. Next, under the protection of nitrogen gas, the graphene and magnesium carbonate powders were added to a continuous screw reaction extruder, the temperature of the continuous screw reaction extruder was set to 300°C, the extrusion pressure was 20 MPa, and aniline chloride The acid salt and magnesium carbonate are decomposed by heat, and the decomposed carbon dioxide and ammonia gas ...
Embodiment 3
[0027] Put 500g of expanded graphite into 1000g concentration of phenyl quaternary ammonium chlorate electrolyte solution of 20 mg / L, let stand for 1 day, allow the cations in the electrolyte solution to infiltrate between the graphite material layers to form intercalated graphite, filter Isolate and take out described intercalated graphite, put 250g intercalated graphite and 2.5g magnesium carbonate blend into continuous screw reaction extruder, obtain extruded solid product, adopt sieve hole to screen out particle diameter and be the graphene of 50~60nm and Magnesium carbonate powder. Next, under the protection of nitrogen gas, add graphene and magnesium carbonate powder into the continuous screw reaction extruder, set the temperature of the continuous screw reaction extruder to 300 ° C, extrusion pressure 20 MPa, phenyl quaternary ammonium The chlorate and magnesium carbonate are thermally decomposed, and the decomposed carbon dioxide and ammonia gas are released to obtain ...
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