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Textile wastewater treatment agent and preparation method and application thereof

A technology of textile wastewater and treatment agent, which is applied in the textile industry wastewater treatment, water/sewage treatment, water/sludge/sewage treatment and other directions, can solve the problems of strong corrosion of equipment, poor treatment effect, poor decolorization effect, etc. Achieve the effect of low production cost, good decolorization effect and fast coagulation effect

Inactive Publication Date: 2017-01-11
刘可
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In the prior art, the textile wastewater is mainly treated with a single iron salt and aluminum salt as a chemical flocculant. The dosage is large and the decolorization effect is poor. Not only the treatment effect is not good, but also it is highly corrosive to the equipment.

Method used

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  • Textile wastewater treatment agent and preparation method and application thereof

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Effect test

Embodiment 1

[0016] In the embodiment of the present invention, a textile wastewater treatment agent is composed of the following raw materials in parts by weight: 8 parts of acrylic acid, 5 parts of tetrabutylurea, 12 parts of longan shell, 25 parts of kaolin, and 1 part of diphenylmethane diisocyanate .

[0017] Mix acrylic acid with a 75% ethanol solution 6 times its mass to prepare an acrylic acid solution; crush longan shells, pass through a 150-mesh sieve, add acrylic acid solution, soak at 65°C for 4.5h, then raise the temperature to 85°C and Heat and stir for 120 minutes to obtain the longan shell material. Grind kaolin and pass through a 150-mesh sieve, then add tetrabutylurea and stir for 40 minutes, then raise the temperature to 60°C and stir at this temperature for 20 minutes, then add longan shell materials, stir at 75°C for 25 minutes, and then add diphenylmethane Diisocyanate was stirred at 70°C for 20 minutes, then microwaved for 20 minutes, the microwave power was 700W, t...

Embodiment 2

[0019] In the embodiment of the present invention, a textile wastewater treatment agent is composed of the following raw materials in parts by weight: 15 parts of acrylic acid, 12 parts of tetrabutylurea, 20 parts of longan shell, 33 parts of kaolin, and 5 parts of diphenylmethane diisocyanate .

[0020] Mix acrylic acid with a 75% ethanol solution 6 times its mass to prepare an acrylic acid solution; crush longan shells, pass through a 150-mesh sieve, add acrylic acid solution, soak at 65°C for 4.5h, then raise the temperature to 85°C and Heat and stir for 120 minutes to obtain the longan shell material. Grind kaolin and pass through a 150-mesh sieve, then add tetrabutylurea and stir for 50 minutes, then raise the temperature to 60°C and stir at this temperature for 30 minutes, then add longan shell materials, stir at 75°C for 30 minutes, and then add diphenylmethane Diisocyanate was stirred at 70°C for 30 minutes, then microwaved for 20 minutes, the microwave power was 700W...

Embodiment 3

[0022] In the embodiment of the present invention, a textile wastewater treatment agent is composed of the following raw materials in parts by weight: 10 parts of acrylic acid, 7 parts of tetrabutylurea, 14 parts of longan shell, 27 parts of kaolin, and 2 parts of diphenylmethane diisocyanate .

[0023] Mix acrylic acid with a 75% ethanol solution 6 times its mass to prepare an acrylic acid solution; crush longan shells, pass through a 150-mesh sieve, add acrylic acid solution, soak at 65°C for 4.5h, then raise the temperature to 85°C and Heat and stir for 120 minutes to obtain the longan shell material. Grind kaolin, pass through a 150-mesh sieve, then add tetrabutylurea and stir for 40-50 minutes, then raise the temperature to 60°C and stir at this temperature for 25 minutes, then add longan shell materials, stir at 75°C for 28 minutes, and then add diphenyl Methyl methane diisocyanate and stirred at 70°C for 25min, then microwaved for 20min with a microwave power of 700W, ...

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Abstract

The invention discloses a textile wastewater treatment agent and a preparation method and application thereof. The textile wastewater treatment agent is composed of, by weight, 8-15 parts of acrylic acid, 5-12 parts of tetrabutyl urea, 12-20 parts of longan shell, 25-33 parts of kaolin and 1-5 parts of diphenylmethane diisocyanate. The preparation method includes: smashing the longan shell, using a prepared acrylic acid solution for soaking, and thermally stirring to obtain a longan shell material; grinding kaolin, adding tetrabutyl urea, stirring, adding the longan shell material, stirring, adding diphenylmethane diisocyanate, stirring, and performing microwave treatment, high-temperature calcining and cooling to room temperature to obtain. The treatment agent is used for treating textile printing and dyeing wastewater and is quick in condensation, good in decoloring effect, high in activity, free of secondary pollution, low in dosage, convenient to use, suitable for the textile wastewater having big change in water quality and good in acid-resistant heat-resistant performance. The treatment agent is extensive in raw material source, low in production cost and free of corrosion of and damage to equipment, and the preparation method is simple in process, easy to operate and suitable for industrial production.

Description

technical field [0001] The invention relates to the technical field of sewage treatment, in particular to a textile wastewater treatment agent and its preparation method and application. Background technique [0002] Textile wastewater is mainly wastewater containing organic matter such as natural impurities, fat, and starch produced during the cooking, rinsing, bleaching, and sizing of raw materials. Printing and dyeing wastewater is produced in multiple processes such as washing and dyeing, printing, and sizing. It contains a large amount of organic matter such as dyes, starch, cellulose, lignin, and detergent, as well as inorganic matter such as alkali, sulfide, and various salts. very strong. Wastewater is characterized by high concentration of organic matter, complex composition, deep and changeable color, large pH changes, and large changes in water quantity and quality. It is a difficult-to-treat industrial wastewater. With the development of chemical fiber fabrics,...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C02F1/00C02F1/52C02F1/54C02F103/30
CPCC02F1/00C02F1/52C02F1/54C02F2103/30
Inventor 不公告发明人
Owner 刘可
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