Insect-repelling waterborne wood coating
A wood coating, water-based technology, applied in the field of coatings, can solve the problems of volatile solvent waste, short extraction time, pyrethrin degradation, etc., and achieve the effects of high efficiency, stability, high extraction rate, and conventional equipment.
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Embodiment 1
[0028] (1) After drying 400g of pyrethrum petals at 100°C for 30 minutes, crush them through an 80-mesh sieve to obtain 260g of pyrethrum flower powder;
[0029] (2) Put 200g of pyrethrum flower powder, 10g of cellulase, 1176g of ethyl acetate and 824g of n-octane in a Soxhlet extractor, heat to reflux, and at the same time irradiate with ultraviolet light for 50min, continue to reflux for 5 hours and take The extract is ready for use;
[0030] (3) Distill the extract to collect 1004g of 75~80℃ distillate as ethyl acetate, 792g of 122~130℃ distillate as n-octane, and the rest as pyrethrins with a weight of 7.7g.
[0031] (4) 6g pyrethrins were dissolved in 30g ethanol to obtain 36g pyrethrin-ethanol solution, 10g chitosan was dissolved in 200g 3wt% acetic acid aqueous solution to obtain 210g chitosan aqueous solution, and 36g pyrethrin-ethanol solution The solution is uniformly mixed with 210 g of chitosan aqueous solution, and spray-dried to obtain 15.6 g of pyrethrin-loaded...
Embodiment 2
[0034] (1) After drying 400g of pyrethrum petals at 105°C for 25 minutes, crush them through a 90-mesh sieve to obtain 250g of pyrethrum flower powder;
[0035] (2) Put 200g of pyrethrum flower powder, 14g of cellulase, 1600g of ethyl acetate and 800g of n-octane in a Soxhlet extractor, heat to reflux, and at the same time irradiate with ultraviolet light for 40min, continue to reflux for 6 hours and take The extract is ready for use;
[0036] (3) Distill the extract to collect 1440g of 75~80℃ distillate as ethyl acetate, 744g of 122~130℃ distillate as n-octane, and the remainder as pyrethrins with a weight of 8.04g.
[0037] (4) Dissolve 6g pyrethrins in 24g ethanol to obtain 30g pyrethrin-ethanol solution, dissolve 10g chitosan in 150g 3wt% acetic acid aqueous solution to obtain 160g chitosan aqueous solution, and dissolve 30g pyrethrin-ethanol The solution is uniformly mixed with 150 g of chitosan aqueous solution, and spray-dried to obtain 14.8 g of pyrethrin-loaded chito...
Embodiment 3
[0040] (1) After drying 400g of pyrethrum petals at 110°C for 20 minutes, crush them through a 100-mesh sieve to obtain 244g of pyrethrum flower powder;
[0041] (2) Put 200g of pyrethrum flower powder, 16g of cellulase, 1666g of ethyl acetate and 1334g of n-octane in a Soxhlet extractor, heat to reflux, and at the same time irradiate with ultraviolet light for 60min, continue to reflux for 4 hours and take The extract is ready for use;
[0042](3) Distill the extract to collect 1600g of 75~80℃ distillate as ethyl acetate, 1282g of 122~130℃ distillate as n-octane, and the remainder as pyrethrins, weighing 7.89g.
[0043] (4) 6g pyrethrins were dissolved in 36g ethanol to obtain 42g pyrethrin-ethanol solution, 10g chitosan was dissolved in 180g 3wt% acetic acid aqueous solution to obtain 190g chitosan aqueous solution, and 36g pyrethrin-ethanol solution The solution was uniformly mixed with 144 g of chitosan aqueous solution, and spray-dried to obtain 13.2 g of pyrethrin-loade...
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