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463results about How to "Promote rupture" patented technology

Large phase ratio liquid-liquid two-phase continuous extraction apparatus

ActiveCN102512848APrevent backmixingImproved stage efficiency for unit mass transfer heightsLiquid solutions solvent extractionPhase ratioEngineering
A large phase ratio liquid-liquid two-phase continuous extraction apparatus belongs to the field of liquid-liquid extraction and separation. The apparatus contains a tower body, a gas buffer chamber, a liquid film aggregation device, liquid film dispersers, a liquid film distributor, an air-pressure chamber and the like. The liquid film dispersers and the liquid film distributor can be combined together to realize dispersion of small-volume organic phase by the use of tiny bubbles, thus solving the problem that it is not easy to fully disperse small-volume organic phase by a traditional stirring mode. The phase ratio of a light phase to a heavy phase flowing upstream in the tower body can be adjusted by the interlayer gap of the liquid film distributor. The light phase and the heavy phase can be operated by counter current under the condition of super-large phase ratio. A liquid film disperser and a bubble connection cap are arranged at intervals in the tower body, so as to realize repeated coagulation and dispersion of rising bubbles and achieve high stage efficiency of height of mass transfer unit. A liquid film aggregation device on the top of the tower can be used for bubble coagulation and demulsification and is suitable for extraction operation of an easily-emulsified system. The apparatus provided by the invention is applicable to continuous countercurrent operation under the condition of multi-stage series connection.
Owner:INST OF PROCESS ENG CHINESE ACAD OF SCI

Multiple-magnetron type large-capacity microwave-assisted extraction machine and microwave-assisted extraction method thereof

The invention discloses a multiple-magnetron type large-capacity microwave-assisted extraction machine and a microwave-assisted extraction method thereof, belonging to the field of biological raw material extraction equipment and an extraction method. The multiple-magnetron type large-capacity microwave-assisted extraction machine comprises a rack, a transmission device, a microwave tank, a microwave device, an air-entrapping device, a rotor device, a discharging device and a control device, wherein a plurality of magnetron installing holes uniformly and equidistantly distributed are formed in the wall of the microwave tank; the microwave device comprises a plurality of high-frequency magnetrons which are uniformly and equidistantly arranged on the wall of the microwave tank, and the high-frequency magnetrons are connected with an external power source; the air-entrapping device comprises a plurality of compressed air inlets formed in the wall of the microwave tank, a compressed air input pipeline and a plurality of electromagnetic valves; the rotor device comprises a rotating shaft and a plurality of stirring wings which are fixed on the rotating shaft and form certain crossing angles with the rotating shaft. The multiple-magnetron type large-capacity microwave-assisted extraction machine has the advantages that feed liquid in the microwave tank continuously runs and interchanges, an extractive is uniformly subjected to the action of an electromagnetic field to be heated, the extraction rate is increased, and the extraction time is shortened.
Owner:永州中农银杏开发有限责任公司

Method for extracting bamboo polysaccharides

The invention relates to methods for efficiently extracting and separating bamboo polysaccharides, belonging to the technical field of plant effective ingredient separated preparation. The invention discloses a method for extracting bamboo polysaccharides. The method comprises the following sequential steps: (1) pretreating bamboos, which serve as raw materials, by adopting a steam explosion method, so as to obtain a bamboo material subjected to steam explosion treatment; (2) carrying out water extraction on the bamboo material subjected to steam explosion treatment, so as to obtain a bamboo water extract; (3) carrying out concentrating refinement on the bamboo water extract by adopting any way as follows: a way I, namely carrying out vacuum concentration on the bamboo water extract, and then, carrying out alcohol precipitation treatment, thereby obtaining a bamboo polysaccharide product; a way II, namely carrying out concentrating refinement on the bamboo water extract by directly adopting a membrane separation method, thereby obtaining the bamboo polysaccharide product. According to the steam explosion method in the step (1), the bamboos are subjected to instantaneous explosion after the bamboos are subjected to pressure maintaining for 30-240 seconds under the pressure of 1.4-3.0MPa, and the explosion time T is not shorter than 0.005075 second and not longer than 0.008752 second.
Owner:ZHEJIANG UNIV

Device for continuously and rapidly defoaming high-viscosity fluid

The invention relates to a device for continuously and rapidly defoaming high-viscosity fluid. The upper part of the device is a vacuum defoaming tank; a vacuum suction opening is arranged on the vacuum defoaming tank, and an umbrella-shaped piece is arranged in the vacuum defoaming tank; the upper part of the umbrella-shaped piece is narrower than the lower part and is connected with a feeding inlet; the position where the upper part of the umbrella-shaped piece is connected with the feeding inlet is provided with a slit and a slit adjusting device; the fluid of different viscosity and flow rate, which enters the vacuum defoaming tank, can form continuous films of uniform thickness on the umbrella-shaped piece by adjusting the width of the slit; the lower part of the device is a screw extruder which is provided with a motor and a driving device; the motor rotates to drive a screw to rotate so as to continuously output the material in the vacuum defoaming tank; in addition, a stirring device can be arranged in the vacuum defoaming tank according to the need, and the stirring device can be driven by the screw at the bottom or other driving force on the top of the vacuum defoaming tank. The device can be used for continuously and rapidly defoaming the high-viscosity fluid, particularly the high-viscosity fluid whose characteristic can change along with time, temperature and other factors.
Owner:CHINA BLUESTAR CHENGRAND CO LTD

Method for extracting toosendanin from cortex meliae

The invention relates to a method for extracting toosendanin from cortex meliae. The method comprises the following processing steps: cleaning dry mature cortex meliae and then crushing the mature cortex meliae by a pulverizer, grinding the mature cortex meliae into powder, drying the powder and adding a 60% ethanol solvent; adjusting the pH value of the solution to 4-6, and adding cellulase for enzymolysis; putting the extracting solution into a double-frequency ultrasonic extractor to obtain an enzymatic hydrolysate; carrying out high-temperature inactivation on the enzymatic hydrolysate to obtain an extracting solution; centrifuging, taking supernate, extracting by use of chloroform, and drying by use of anhydrous sodium sulfate; carrying out suction filtration, concentrating, adding ethanol and heating for dissolving; dropping petroleum ether until the mixture becomes a turbid matter; stewing for separating out a flavescent solid, namely the toosendanin. According to the method, the cortex meliae is taken as the raw material; the stacking effect of enzymolysis and a double-frequency ultrasonic wave is fully utilized; the toosendanin in the cortex meliae is dissolved to the greatest extent; the high-purity toosendanin can be obtained by virtue of extraction and crystallization. The method has the advantages of being simple in equipment, low in extraction cost, high in extraction efficiency, mild in reaction condition, less in solvent consumption, free of pollution and the like.
Owner:NANJING TONGZE AGRI SCI & TECH
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