Preparation method of plant-derived natural food antioxidant
A technology of natural food and antioxidant, which is applied in food ingredients as antioxidant, food preservation, food science, etc. It can solve the problems of large toxic and side effects, poor thermal stability, poor antibacterial effect, etc., and achieve easy processing and preservation, antibacterial High oxidation efficiency and good thermal stability
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example 1
[0019] Weigh 80g of fresh shallots, put them into a tissue breaker, smash them into pulp, and obtain the shallot slurry, add the shallot slurry to 800mL of hydrochloric acid with a mass fraction of 0.2%, stir and mix at 300r / min, and adjust the pH with citric acid 2.0 to obtain a mixed solution, put the mixed solution into a high-voltage pulse electric field extraction device and extract for 3 hours, control the number of pulses to 10, and the field strength is 15kV / cm, transfer it to a centrifuge, and centrifuge at 12000r / min for 15 minutes to obtain Acid extraction solution and precipitation; add the above precipitation into 800mL disodium hydrogen phosphate-citric acid buffer solution with a pH of 7.5, stir and mix evenly at 200r / min, and put it into a high-voltage pulse electric field extraction device for extraction for 2h, and control the number of pulses to 8 1, the field strength is 18kV / cm, and the mixed material liquid is obtained, and the mixed material liquid is suc...
example 2
[0022] Weigh 90g of fresh shallots, put them into a tissue breaker, smash them into pulp, and obtain the shallot slurry, add the shallot slurry to 900mL of hydrochloric acid with a mass fraction of 0.3%, stir and mix evenly at 350r / min, and adjust the pH with citric acid 2.2, to obtain a mixed solution, put the mixed solution into a high-voltage pulse electric field extraction device for extraction for 3.5 hours, control the number of pulses to 11, and the field strength is 16kV / cm, transfer it to a centrifuge, and centrifuge at 13000r / min for 18 minutes, Obtain acid extract and precipitate; add the above precipitate into 900mL disodium hydrogen phosphate-citric acid buffer solution with a pH of 7.5, stir and mix evenly at 250r / min, and put it into a high-voltage pulse electric field extraction device for extraction for 2.5h, control the number of pulses 9, the field strength is 19kV / cm, to obtain the mixed feed solution, and the mixed feed solution is suction-filtered to obtai...
example 3
[0025] Weigh 100g of fresh shallots, put them into a tissue breaker to crush and make pulp, and then add shallot pulp to 1000mL of hydrochloric acid with a mass fraction of 0.4%, stir and mix evenly at 400r / min, and adjust the pH with citric acid 2.5 to obtain a mixed solution, put the mixed solution into a high-voltage pulse electric field extraction device and extract for 4 hours, control the number of pulses to 12, and the field strength is 18kV / cm, transfer it to a centrifuge, and centrifuge at 15000r / min for 20 minutes to obtain Acid extraction solution and precipitation; add the above precipitation into 1000mL disodium hydrogen phosphate-citric acid buffer solution with a pH of 7.5, stir and mix evenly at 300r / min, and put it into a high-voltage pulse electric field extraction device for extraction for 3h, and control the number of pulses to 10 1, the field strength is 20kV / cm, to obtain the mixed material liquid, and the mixed material liquid is suction-filtered to obtai...
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