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Adamantine mono-quaternary ammonium salt cationic three compound combination flooding produced water oil remover

A quaternary ammonium salt cation and ternary composite technology, which is applied in the field of adamantane single quaternary ammonium cation type three-component compound flooding degreasing agent, can solve the problems of high cost and difficult regeneration, and achieve excellent temperature resistance, Effect of high oil removal efficiency and strong interface modification function

Active Publication Date: 2017-02-01
安徽创宇新材料科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The most common adsorbent is activated carbon, which has good adsorption performance for oil, but it is expensive and difficult to regenerate. It is generally only used for advanced treatment of oily sewage

Method used

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  • Adamantine mono-quaternary ammonium salt cationic three compound combination flooding produced water oil remover
  • Adamantine mono-quaternary ammonium salt cationic three compound combination flooding produced water oil remover
  • Adamantine mono-quaternary ammonium salt cationic three compound combination flooding produced water oil remover

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0029] Embodiment 1: Degreaser BD 1 and its preparation method

[0030] (1) Degreaser BD 1 The composition and its components are as follows:

[0031]

[0032] According to existing literature, the preparation method of described adamantane monoquaternary ammonium salt cationic surfactant is as follows:

[0033]

[0034] (2) Degreaser BD 1 The preparation method is as follows:

[0035] ① Mix 20 parts of adamantane monoquaternary ammonium cationic surfactant and 5 parts of sodium carboxymethylcellulose into the first beaker, add 40 parts of water, heat while stirring, the stirring rate is 250ppm, and the heating temperature 40°C, the heating time is 20min, after the heating time is over, the temperature is naturally cooled to room temperature to obtain the mixed solution A;

[0036] ② Mix 10 parts of 4A zeolite and 15 parts of hydrogenated tallow alcohol polyoxyethylene (11) ether into the second beaker, add 40 parts of water, and heat while stirring. The stirring ra...

Embodiment 2

[0038] Embodiment 2: Degreaser BD 2 and its preparation method

[0039] (1) Degreaser BD 2 The composition and its components are as follows:

[0040]

[0041] According to existing literature, the preparation method of described adamantane monoquaternary ammonium salt cationic surfactant is as follows:

[0042]

[0043] (2) Degreaser BD 2 The preparation method is as follows:

[0044] ① Mix 20 parts of adamantane monoquaternary ammonium salt cationic surfactant and 8.5 parts of sodium carboxymethylcellulose into the first beaker, add 50 parts of water, heat while stirring, the stirring rate is 300ppm, and the heating temperature 42°C, the heating time is 30min, after the heating time is over, the temperature is naturally cooled to room temperature to obtain the mixed solution A;

[0045] ② Mix 16 parts of 4A zeolite and 22 parts of hydrogenated tallow alcohol polyoxyethylene (11) ether into the second beaker, add 50 parts of water, and heat while stirring. The stirri...

Embodiment 3

[0047] Embodiment 3: Degreaser BD 3 and its preparation method

[0048] (1) Degreaser BD 3 The composition and its components are as follows:

[0049]

[0050] According to existing literature, the preparation method of described adamantane monoquaternary ammonium salt cationic surfactant is as follows:

[0051]

[0052] (2) Degreaser BD 3 The preparation method is as follows:

[0053] ① Mix 20 parts of adamantane monoquaternary ammonium salt cationic surfactant and 12.5 parts of sodium carboxymethylcellulose into the first beaker, add 55 parts of water, heat while stirring, the stirring rate is 320ppm, and the heating temperature 43°C, the heating time is 25min, after the heating time is over, the temperature is naturally cooled to room temperature to obtain the mixed solution A;

[0054] ② Mix 12 parts of 4A zeolite and 26 parts of hydrogenated tallow alcohol polyoxyethylene (11) ether into the second beaker, add 55 parts of water, and heat while stirring. The sti...

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Abstract

The invention belongs to the technical field of oil field wastewater treatment, and particularly relates to an adamantine mono-quaternary ammonium salt cationic three compound combination flooding produced water oil remover, which is prepared from compounding an adamantine mono-quaternary ammonium salt cationic surface active agent, 4A zeolite, sodium carboxymethylcellulose, alcohol polyoxyethylene hydrogenated butter (11) ether and water. The adamantine mono-quaternary ammonium salt cationic surface active agent is a molecule with a long carbon chain alkyl non-polar group and an adamantyl polar group. The oil remover provided by the invention has the characteristics of simple preparation process, low cost, high temperature resistance and salt tolerance performances and good oil removing effect, the temperature resistance achieves 240 DEG C, the salinity tolerance degree achieves 240,000mg / L, and the oil removal rate reaches 97 percent or above and is improved by not less than 50 percent compared with an existing medicament. Therefore, the adamantine mono-quaternary ammonium salt cationic three compound combination flooding produced water oil remover provided by the invention can be applied in an oil removal process of three compound combination flooding produced water.

Description

technical field [0001] The invention relates to a degreasing agent for oil field sewage treatment, in particular to an adamantane monoquaternary ammonium salt cationic three-element compound flooding produced water degreasing agent. Background technique [0002] With the continuous development of oilfields and the continuous development of oil recovery technology, it has experienced primary, secondary, and tertiary oil recovery. Some oil fields in my country have entered the stage of tertiary oil recovery. Common tertiary oil recovery methods include polymer flooding, ASP flooding, binary flooding (alkali-polymer flooding, ie AP flooding), alkali flooding, foam composite flooding, etc. The composite flooding recovery technology is the most typical. Relevant studies have shown that ASP flooding can significantly increase oil recovery and has broad application prospects. However, because the produced water of ASP flooding contains a large amount of polyacrylamide, surfactant...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C02F1/00C02F1/28C02F1/42C02F1/56C02F103/10
CPCC02F1/00C02F1/281C02F1/285C02F1/42C02F1/56C02F2103/10C02F2305/04
Inventor 刘亭亭
Owner 安徽创宇新材料科技有限公司
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