A kind of bispyribac-cyhalofop-butyl suspoemulsion and preparation method thereof

A technology of cyhalofop-fop and bispyribac, which is applied in the field of bispyribac-cyhalofop-emulsion suspoemulsion and its preparation, can solve problems such as delamination instability, environmental pollution, and influence on drug efficacy, and achieve improved safety and efficacy, improve weed control effect, improve the effect of utilization

Active Publication Date: 2019-12-06
祥霖美丰生物科技(淮安)有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, after research, these dosage forms all have the problem of low control effect
At the same time, the existing wettable powders of bispyriben and cyhalofop in China will produce dust during production and use, which will cause pollution to the environment and people; , delamination and other unstable phenomena seriously affect the drug efficacy; bispyribac and cyhalofop-ethyl EC contain a large amount of harmful solvents, which seriously pollute the environment; too high

Method used

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  • A kind of bispyribac-cyhalofop-butyl suspoemulsion and preparation method thereof
  • A kind of bispyribac-cyhalofop-butyl suspoemulsion and preparation method thereof
  • A kind of bispyribac-cyhalofop-butyl suspoemulsion and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0037] After adding 150# solvent naphtha 150g in the shear kettle, then add 156.3g of the former medicine of cyhalofop-ethyl (effective content 96%), emulsifier alkylphenol polyoxyethylene (9) ether 10g, wetting agent dodecane Calcium phenyl sulfonate 10g, fatty alcohol polyoxyethylene ether 10g, dispersant sodium lignosulfonate 20g, after mixing and stirring until transparent, add 550.1g of deionized water while stirring, then add bispyribac Content 96%) 52.1g, thickening agent xanthan gum 10g, antifreeze agent ethylene glycol 30g, long-chain alcohol defoamer 0.5g and pH regulator sodium acetate 1g, mix, stir, in high-speed shearing machine 1500~10000 Cut for 10 to 40 minutes at the speed of rpm, and then grind to particle size D with a sand mill 90 When the thickness is smaller than 3 μm, the suspoemulsion of bispyribac and cyhalofop-fop is prepared.

Embodiment 2

[0039]After adding 150g of 200# solvent oil in the shearing kettle, add 156.3g of the former drug of cyhalofop-ethyl (effective content 96%), emulsifier castor oil polyoxyethylene (10) ether 25g, wetting agent alkyl succinic acid Sodium fat sulfonate 35g, dispersant (NNO) 35g, after mixing and stirring until transparent, add 508.1g of deionized water while stirring, then add 52.1g of bispyribac-ether technical (effective content 96%), thickener silicon 7.5g of magnesium aluminum oxide, 20g of antifreeze glycerin, 1g of polyglycerin defoamer and 10g of pH regulator triethanolamine, mix and stir, and cut 10 to 40 Minutes, and then grind to particle size D by sand mill 90 When the thickness is smaller than 3 μm, the suspoemulsion of bispyribac and cyhalofop-fop is prepared.

Embodiment 3

[0041] After adding turpentine-based vegetable oil 150g in the shear kettle, add the former medicine of cyhalofop-ester (effective content 96%) 156.3g, emulsifier phenylethylphenol polyoxyethylene ether 25g, wetting agent alkyl sulfosuccinate Sodium phosphate 35g, dispersant alkylphenol polyoxyethylene ether phosphate 15g, polycarboxylate 20g, after mixing and stirring until transparent, add 508.1g of deionized water while stirring, then add the former medicine of bispyribacin (effective content 96%) 52.1g, thickener xanthan gum 2g, magnesium aluminum silicate 5.5g, antifreeze agent ethylene glycol 20g, organosilicon type defoamer 1g and pH adjuster triethanolamine 10g, mix, stir, in high speed shear Cutting machine at 1500-10000 rev / min for 10-40 minutes, then grind to particle size D by sand mill 90 When the thickness is smaller than 3 μm, the suspoemulsion of bispyribac and cyhalofop-fop is prepared.

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Abstract

The invention especially relates to a bispyribac sodium-cyhalofop butyl suspoemulsion and a preparation method thereof, belonging to the technical field of pesticides. The bispyribac sodium-cyhalofop butyl suspoemulsion comprises, by mass, 5 to 10% of bispyribac sodium, 15 to 20% of cyhalofop butyl, 1 to 5% of an emulsifier, 2 to 5% of a wetting agent, 2 to 5% of a dispersing agent, 0.5 to 1% of a thickening agent, 2 to 3% of an anti-freezing agent, 0.05 to 0.3% of an antifoaming agent, 0.1 to 1.5% of a pH value adjusting agent and 15 to 20% of an organic solvent, with the balance being water. According to the invention, a scientific ratio of surfactants (including the emulsifier, the wetting agent and the dispersing agent) is employed, so the physical and chemical stability of the ispyribac sodium-cyhalofop butyl suspoemulsion is improved, the utilization rate of the ispyribac sodium-cyhalofop butyl suspoemulsion is increased, and the weeding efficacy of the ispyribac sodium-cyhalofop butyl suspoemulsion is enhanced. The suspoemulsion provided by the invention is prepared through compounding of ispyribac sodium and cyhalofop butyl, has high cost performance, a wide weed control spectrum and fast action, does no harm to later crops and is a novel high-efficiency dosage form of herbicide for rice field.

Description

technical field [0001] The invention relates to the technical field of pesticides, in particular to a bispyribac-cyhalofop-emulsion suspoemulsion and a preparation method thereof. Background technique [0002] Rice is not only the most important food crop in my country, but also one of the main food crops in the world. Nearly half of the world's population, including almost all of East and Southeast Asia, eat rice. Production is on every continent except Antarctica. In the late last century, the average annual rice output in the world was about 400 billion kilograms, and the planting area was about 145 million hectares. The sown area of ​​rice in my country accounts for 1 / 4 of the national grain crops, about 35 million hectares per year, while the output accounts for more than half. Regardless of planting area and output, rice ranks first among my country's grain crops. [0003] And the paddy fields of all rice-growing regions in my country have always had a large amount...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): A01N25/04A01N25/30A01N43/54A01N39/04A01P13/00
CPCA01N25/04A01N25/30A01N39/04A01N43/54A01N2300/00
Inventor 倪登辉黄坚慧周省金毕立国王本上黄挺陈瑜
Owner 祥霖美丰生物科技(淮安)有限公司
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