Gracilaria lemaneiformis extract product and preparation method and application thereof
A technology of extract and asparagus, which is applied in the field of asparagus extract and its preparation, can solve the problems that the extract is difficult to separate and purify, limit the biological activity of asparagus, and the active ingredients are easily destroyed, so as to reduce the harm to the human body. The effect of harm, less impurities, and short extraction time
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Embodiment 1
[0028] Example 1 Preparation of asparagus extract by ultrasonic extraction process
[0029] A preparation method of asparagus extract, comprising the steps of:
[0030] (1) Preparation of novel ionic liquid 1-butyl-3-methylimidazolium bromide: add N- Methylimidazole and brominated n-butane, with toluene as solvent, under nitrogen protection, add stirring reaction, the stirring speed is 300 rpm, the reaction temperature is 65 °C; after the reaction is completed, cool to room temperature, and the lower layer is yellow viscous Thick 1-butyl-3-methylimidazolium bromide crude product, discard the upper layer solution, first wash twice with ethyl acetate to remove unreacted n-butane bromide, then remove ethyl acetate by rotary evaporation and vacuum dry After 24 hours, the pure product of 1-butyl-3-methylimidazolium bromide, which is a novel ionic liquid, was obtained;
[0031] (2) Ultrasonic extraction of asparagus extract: first take asparagus powder in a beaker, and add the nov...
Embodiment 2
[0032] Example 2 Application of asparagus extract
[0033] An active lead compound for free radical scavenging activity in the fields of marine innovative new drugs, seaweed folk medicines, etc. as a kind of asparagus extract; in particular, it is used for scavenging DPPH free radicals, hydroxyl free radicals ( OH) and superoxide ions ( o 2- ).
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