Moisturizing and water-replenishing soluble cleansing paper and preparation method thereof
A technology of soluble cleansing paper, applied in skin care preparations, pharmaceutical formulations, cosmetic preparations, etc., can solve problems such as easy adhesion, easy cracking and falling apart of cleansing paper, and achieve skin moisture retention, portability, and skin-friendly good sex effect
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Embodiment 1
[0036] Embodiment 1, the preparation of soluble anionic starch
[0037] Described soluble anionic starch is made by following steps:
[0038] S1) Enzymolysis: Take pea starch, add a certain amount of citric acid-disodium hydrogen phosphate buffer solution, stir and gelatinize in a boiling water bath, take it out, constant volume, prepare a gelatinized starch solution of 20mg / ml, and keep the temperature at 45°C Shake in a water bath for 10 minutes, add α-amylase, enzymatically hydrolyze for 80 minutes, stop the reaction to obtain starch hydrolyzate, and set aside;
[0039] S2) Cross-linking: Add soybean oil, sodium hydroxide solution, Span-80 and epichlorohydrin to the above starch enzymatic hydrolysis solution, stir and mix, wherein, soybean oil, sodium hydroxide solution, Span-80 and epoxy The weight ratio of chloropropane is 1:1:0.2:0.5;
[0040] S3) Anionization: add ethanol solution, monochloroacetic acid, sodium hydroxide solution and the starch enzymatic solution tre...
Embodiment 2
[0042] Embodiment 2, the preparation of cationic nano-microcrystalline cellulose
[0043] The cationic nano-microcrystalline cellulose is prepared by the following steps:
[0044] Take microcrystalline cellulose, crush it, pass through a 20-mesh sieve, add 150ml of 45wt% hydrochloric acid at 45°C, stir, react for 40min, add 9 times the volume of deionized water to dilute to terminate the reaction, and use deionized water to dilute the obtained product repeatedly. Centrifuge and wash to pH 5.0; put the obtained product into a dialysis bag, use flowing deionized water to dialyze the paper to a constant pH value, and treat the dialyzed suspension with an ultrasonic oscillator for 10 minutes to obtain nanocrystalline cellulose suspension liquid, in order to avoid product aggregation due to heat, the treatment is carried out in a hot water bath;
[0045] Add the above-mentioned nano-microcrystalline cellulose suspension to phosphate buffer solution to obtain a nano-microcrystall...
Embodiment 3
[0046] Embodiment 3, the preparation of watermelon rind polypeptide
[0047] The watermelon rind polypeptide is prepared by the following steps:
[0048] Take the dried medicinal material from watermelon rind, wash, crush, and sieve to obtain a fine powder. Take the above fine powder, add 8 times the amount of 30% ethanol solution to the fine powder, soak for 1 hour, extract in a constant temperature water bath at 70°C for 1.0 hour, and filter. Instantly.
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