Preparation method of antimicrobial coating of implantable medical device
A technology for medical devices and antibacterial coatings is applied in the field of preparation of antibacterial coatings to achieve the effects of simple preparation process, increased contact area, and easy large-scale production
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Embodiment 1
[0049] Such as Figure 1-Figure 6 Shown, the invention provides the preparation method of the antibacterial coating of implantable medical device, comprises the steps:
[0050] S1: Soak the implantable medical device 1 in a solution containing dopamine for treatment, take it out and dry it with nitrogen at room temperature for later use, and obtain a surface-treated implantable medical device 2;
[0051] S2: Put the mask plate 3 on the surface-treated metal part of the implantable medical device 2, and then spray the coating solution on the surface of the implantable medical device;
[0052] S3: remove the mask, wait until the solvent is completely volatilized, and obtain an implantable medical device containing an antibacterial coating 4;
[0053] Wherein, the shape of the mask 3 matches the shape of the metal part of the implantable medical device 1 , and holes are opened on the surface of the mask 3 . Preferably, the mask plate 3 is made of polydimethylsiloxane (PDMS).
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Embodiment 2
[0074] The preparation method of the antibacterial coating of the implantable medical device provided in this example is basically the same as that of Example 1, and only the differences will be described below.
[0075] In this embodiment, the solution containing dopamine in the step S1 is a Tris-HCl solution of dopamine, the pH value of the solution is 8.5, and the concentration of dopamine in the solution is 0.03mol / L. Soak in Tris-HCl solution of dopamine for 6h.
[0076] The mask in the step S2 is made of polydimethylsiloxane (PDMS). The holes on the surface of the mask are square holes with a size of 2mm×2mm and a porosity of 70%.
[0077] The coating solution is composed of medicine, polymer and solvent, and the components of the coating solution are: 1% of medicine, 2% of polymer and 97% of solvent in terms of mass percentage.
[0078]Among them, the drug is preferably rifampicin; the polymer is preferably a copolymer of lactic acid and glycolide; the solvent is prefe...
Embodiment 3
[0082] The preparation method of the antibacterial coating of the implantable medical device provided in this example is basically the same as that of Example 1, and only the differences will be described below.
[0083] In this embodiment, the solution containing dopamine in the step S1 is a Tris-HCl solution of dopamine, the pH value of the solution is 8.5, and the concentration of dopamine in the solution is 0.04mol / L. Soak in Tris-HCl solution of dopamine for 8h.
[0084] The mask in the step S2 is made of polydimethylsiloxane (PDMS), and the holes on the surface of the mask are circular holes with a diameter of 3mm and a porosity of 80%.
[0085] The coating solution is composed of medicine, polymer and solvent. According to mass percentage, the composition of the coating solution is: 3% of medicine, 5% of polymer and 92% of solvent.
[0086] Among them, the drug is preferably cephalosporin; the polymer is preferably polyethylene glycol-polylactic acid-polyglutamic acid ...
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Abstract
Description
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Application Information
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