A traditional Chinese medicine pill for treating diabetic nephropathy and its preparation method and application
A technology for diabetic nephropathy and traditional Chinese medicine pills, applied in the field of medicine, can solve problems such as inability to effectively prevent disease progression, controversial drug application, prone to hyperkalemia, etc., to improve the positive percentage of PAS staining, significantly resist cell oxidation, reduce The effect of renal HE staining on pathological scoring
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[0036] (1) Preparation of traditional Chinese medicine pills
[0037] 1 test material
[0038] 1.1 Instrument
[0039] Traditional Chinese medicine multifunctional extraction and reflux concentration unit (Hunan Jinyifan Pharmaceutical Equipment Industry Co., Ltd., RZZ Xiang-082-06).
[0040] Multifunctional pellet coating machine (Shenzhen Xinyite Technology Co., Ltd., Mini-250).
[0041] 1.2 Raw and auxiliary materials
[0042] Astragalus (Bozhou Huikang Chinese Herbal Pieces Co., Ltd.);
[0043] Radix Puerariae (Bozhou Huikang Chinese Herbal Pieces Co., Ltd.);
[0044] Morus alba (Bozhou Huikang Chinese Herbal Pieces Co., Ltd.);
[0045] Ethanol (produced by Guangdong Shunguan Gas Solvent Co., Ltd.);
[0046] Microcrystalline cellulose (produced by Anhui Shanhe Pharmaceutical Excipients Co., Ltd.);
[0047] Starch (produced by Anhui Shanhe Pharmaceutical Excipients Co., Ltd.);
[0048] Dextrin (produced by Anhui Shanhe Pharmaceutical Excipients Co., Ltd.);
[0049] T...
Embodiment 1
[0052] Take 2.5kg of Radix Astragali, 5.0kg of Pueraria Radix, and 2.5kg of Cortex Mori, add 8 times the amount of 70% ethanol to reflux and extract twice, each time for 3 hours, filter, combine the filtrate, filter with a 50nm ceramic membrane, collect the filtrate, recover the ethanol and concentrate (Temperature: 70°C; Air pressure: -0.8~-0.6MPa) to a relative density of 1.32~1.35 (70°C), collect the paste for later use. Three parts were prepared in the same way: extract 1, extract 2 and extract 3.
[0053] Take the above three batches of extracts, add microcrystalline cellulose, starch and dextrin accounting for 40-60% of the total amount, respectively add 5% talcum powder as anti-sticking agent, mix well, add appropriate amount of water to make soft material, squeeze The process parameters of this step are: extrusion speed 35rpm, spheronization time 4min, spheronization speed 1000rpm. Dry at 60±10°C for 3 hours, pass through 18 and 24 mesh sieves, take the pellets that c...
Embodiment 2
[0056] Take 2.5kg of Radix Astragali, 5.0kg of Pueraria Radix, and 2.5kg of Cortex Mori, add 8 times the amount of 70% ethanol to reflux and extract twice, each time for 3 hours, filter, combine the filtrate, filter with a 50nm ceramic membrane, collect the filtrate, recover the ethanol and concentrate (Temperature: 70°C; Air pressure: -0.8~-0.6MPa) to a relative density of 1.32~1.35 (70°C), collect the paste for later use. Three parts were prepared in the same way: extract 1, extract 2 and extract 3.
[0057] Take the above three batches of extracts, respectively investigate the influence of microcrystalline cellulose, starch and dextrin on the yield of pellets, add 5% talcum powder as an anti-sticking agent, make the drug loading 50%, mix well, add Appropriate amount of water is used to make soft materials, extruded and spheronized into pellets, the process parameters of this step are: extrusion speed 35rpm, spheronization time 4min, spheronization speed 1000rpm. Dry at 60±...
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