Cellular denitrification catalyst and preparation method thereof
A denitrification catalyst, honeycomb technology, applied in the direction of chemical instruments and methods, heterogeneous catalyst chemical elements, physical/chemical process catalysts, etc., can solve the problems of unbalanced active centers, unstable activity, etc., to achieve increased density, The effect of stable catalyst activity and tight connection
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Embodiment 1
[0059] will contain TiO 2 500g of titanyl sulfate is dissolved in the sulfuric acid solution, and the 3 22.5g of ammonium molybdate, as CeO 2 Total 14g of rare earth solution to form TiO 2 It is a 35g / L mixed solution. After stirring for 2 hours, gradually add ammonia water to adjust the pH value to 9.5. After the precipitation is complete, filter and wash; then use deionized water to make a slurry with a water content of 50%, and add V 2 o 5 A total of 12.5g of ammonium metavanadate solution, stirred for 1.5h, dried, roasted at 550°C for 8h, and then ground into a powder with a particle size of less than 20μm; the powder was mixed with MoO 3 A total of 7.5g of ammonium molybdate, 4g of stearic acid, 3g of polyethylene oxide and deionized water are used to make a paste with a water content of 30%, adjust the pH value to 8.5 with ammonia water, add 5g of nano silicon dioxide, 17.5g of glass after stirring Fiber, 4g carboxymethyl cellulose, stirred for 40min, sealed and left...
Embodiment 2
[0063] No pore-forming agent polyethylene oxide is added, and the rest are the same as in Example 2, about to contain TiO 2 500g of titanyl sulfate is dissolved in the sulfuric acid solution, and the 3 22.5g of ammonium molybdate, as CeO 2 A total of 12.5g of rare earth solution to form TiO 2 It is a 30g / L mixed solution. After stirring for 1.5h, gradually add ammonia water to adjust the pH value to 10. After the precipitation is complete, filter and wash; then use deionized water to make a slurry with a water content of 50% from the washed material, and add V 2 o 5 A total of 10g of ammonium metavanadate solution, stirred for 1.5h, dried, roasted at 550°C for 8h, and then ground into a powder with a particle size of less than 30μm; the powder was mixed with MoO 3 The ammonium molybdate of 7.5g, 3.5g stearic acid, 3.5g polyoxyethylene and deionized water are made the paste body containing water 32%, adjust pH value to 8.0 with ammoniacal liquor, add 4.5g nano silicon dioxi...
Embodiment 3
[0067] will contain TiO 2 500g of titanyl sulfate is dissolved in the sulfuric acid solution, and the 3 20g of ammonium molybdate, as CeO 2 A total of 10g of rare earth solution to form a TiO-containing 2 It is a 30g / L mixed solution. After stirring for 1.0h, gradually add ammonia water to adjust the pH value to 9. After the precipitation is complete, filter and wash; then use deionized water to make a slurry with a water content of 45%, and add V 2 o 5 A total of 9g of ammonium metavanadate solution, stirred for 1.0h, dried, roasted at 550°C for 8h, and then ground into a powder with a particle size of less than 15μm; the powder was mixed with MoO 3 The ammonium molybdate of 5g, 3.0g stearic acid, 3.0g polyethylene oxide and deionized water are made into a paste with a water content of 28%, and the pH value is adjusted to 8.2 with ammonia water, and after stirring, add 3.5g nano silicon dioxide, 22.5 g glass fiber, 3g carboxymethyl cellulose, stir for 40min, seal and let...
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