Method for preparing UV light-catalyzed carbon fiber grafted polyaniline
A technology of ultraviolet light and polyaniline, applied in the direction of carbon fiber, fiber processing, textile and papermaking, etc., can solve the problems of poor substrate wettability and high inertia of carbon fiber surface, and achieve the effect of improving electromagnetic wave absorbing performance and enhancing wettability.
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[0020] Example 1:
[0021] A preparation method of UV-light catalyzed chopped carbon fiber grafted polyaniline, the specific preparation steps are as follows:
[0022] Put the chopped carbon fibers with a length of 5 to 20 mm into a reaction system of 0.2 mol / L ammonium persulfate / 0.005 mol / L ferrous chloride, keep at 60 ° C for 2 hours, wash and dry with distilled water, and obtain the oxidized of carbon fiber;
[0023] An appropriate amount of dopamine hydrochloride and tris(hydroxymethylaminomethane) were placed in water, so that the concentration of the prepared dopamine solution was 2 mg / mL, and the pH was adjusted to 8.5 for later use;
[0024] The oxidized carbon fibers are placed in a dopamine solution, reacted for a certain period of time at room temperature of 20-25 °C, washed with anhydrous ethanol for several times, and dried to obtain dopamine-modified chopped carbon fibers, namely: aminated carbon fibers;
[0025] Grafting polyaniline on carbon fiber surface: a...
Example Embodiment
[0028] Example 2:
[0029] A preparation method of UV-light catalyzed chopped carbon fiber grafted polyaniline, the specific preparation steps are as follows:
[0030] Put the chopped carbon fibers with a length of 5 to 20 mm into a reaction system of 0.1 mol / L ammonium persulfate / 0.001 mol / L ferrous chloride, keep it at 70 ° C for 1.5 h, wash and dry with distilled water to obtain oxidized rear carbon fiber;
[0031] An appropriate amount of dopamine hydrochloride and tris(hydroxymethylaminomethane) were placed in water, so that the concentration of the prepared dopamine solution was 3 mg / mL, and the pH was adjusted to 8.5 for later use;
[0032] The oxidized carbon fibers are placed in a dopamine solution, reacted for a certain period of time at room temperature of 20-25 °C, washed with anhydrous ethanol for several times, and dried to obtain dopamine-modified chopped carbon fibers, namely: aminated carbon fibers;
[0033] Grafting polyaniline on the surface of carbon fibe...
Example Embodiment
[0036] Example 3:
[0037] A preparation method of UV-light catalyzed chopped carbon fiber grafted polyaniline, the specific preparation steps are as follows:
[0038] Put the chopped carbon fibers with a length of 5 to 20 mm into a reaction system of 0.15 mol / L ammonium persulfate / 0.003 mol / L ferrous chloride, keep at 80 ° C for 1 h, wash and dry with distilled water, and obtain the oxidized of carbon fiber;
[0039] An appropriate amount of dopamine hydrochloride and tris(hydroxymethylaminomethane) were placed in water, so that the concentration of the prepared dopamine solution was 4 mg / mL, and the pH was adjusted to 8.5 for later use;
[0040] The oxidized carbon fibers are placed in a dopamine solution, reacted for a certain period of time at room temperature of 20-25 °C, washed with anhydrous ethanol for several times, and dried to obtain dopamine-modified chopped carbon fibers, namely: aminated carbon fibers;
[0041] Grafting polyaniline on the surface of carbon fibe...
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