Preparation method and device of photocatalysis thin film
A technology of photocatalytic film and film blowing machine, which is applied in chemical instruments and methods, physical/chemical process catalysts, organic compounds/hydrides/coordination complex catalysts, etc., can solve problems such as not being able to fully utilize TiO, and achieve Good photocatalytic performance, high specific surface area, and the effect of degrading polluted waste
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Embodiment 1
[0024] (1) Put 10kg ferroferric oxide powder into a high-speed mixer and stir at high speed for 3 minutes; add 4.33L n-butyl titanate into the high-speed mixer in 3 times, stir at high speed for 8 minutes, so that it is evenly loaded on the ferroferric oxide On the powder; take out the evenly loaded ferric oxide powder, spread it out, and place it in the air for 10 hours to make it fully hydrolyzed; put the completely hydrolyzed ferric oxide powder in a constant temperature drying oven at 95°C for 10 hours; Put the dry ferric oxide powder into a muffle furnace and calcinate at 450°C for 5 hours to obtain TiO 2 TiO with a load of 10% of the amount of ferric oxide powder 2 Magnetic photocatalyst loaded with Fe3O4.
[0025] (2) Mix 2 kg of foaming agent azodicarbonamide, 0.12 kg of dicumyl peroxide, and 0.5 kg of stearic acid at 100°C, and use an emulsifier to disperse the activated foaming agent obtained by high-speed shearing.
[0026] (3) Add 6kg of the magnetic photocatalys...
Embodiment 2
[0029] (1) Put 10kg ferroferric oxide powder into a high-speed mixer and stir at high speed for 3 minutes; add 4.33L n-butyl titanate into the high-speed mixer in 3 times, stir at high speed for 8 minutes, so that it is evenly loaded on the ferroferric oxide On the powder; take out the evenly loaded ferric oxide powder, spread it out, and place it in the air for 10 hours to make it fully hydrolyzed; put the completely hydrolyzed ferric oxide powder in a constant temperature drying oven at 95°C for 10 hours; Put the dry ferric oxide powder into a muffle furnace and calcinate at 450°C for 5 hours to obtain TiO 2 TiO with a load of 10% of the amount of ferric oxide powder 2Magnetic photocatalyst loaded with Fe3O4.
[0030] (2) Mix 2 kg of foaming agent azodicarbonamide, 0.12 kg of dicumyl peroxide, and 0.5 kg of stearic acid at 100°C, and use an emulsifier to disperse the activated foaming agent obtained by high-speed shearing.
[0031] (3) Add 6kg of the magnetic photocatalyst...
Embodiment 3
[0034] (1) Put 10kg of ferroferric oxide powder into a high-speed mixer and stir at high speed for 3 minutes; add 4.33L of n-butyl titanate into the high-speed mixer in 3 times, and stir at high speed for 10 minutes to make it evenly loaded on the trioxide On the iron powder; take out the evenly loaded ferric oxide powder, spread it out, and place it in the air for 10 hours to make it fully hydrolyzed; put the fully hydrolyzed iron ferric oxide powder in a constant temperature drying oven at 95°C for 10 hours ;Put the dry ferric oxide powder into a muffle furnace and calcinate at 450°C for 5h to obtain TiO 2 TiO with a load of 10% of the amount of ferric oxide powder 2 Magnetic photocatalyst loaded with Fe3O4.
[0035] (2) Mix 2 kg of foaming agent azodicarbonamide, 0.12 kg of dicumyl peroxide, and 0.5 kg of stearic acid at 100°C, and use an emulsifier to disperse the activated foaming agent obtained by high-speed shearing.
[0036] (3) Add 6kg of the magnetic photocatalyst ...
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