High-performance starch-based carbon fiber and preparation method thereof
A starch-based, carbon fiber technology, applied in the direction of fiber chemical characteristics, conjugated rayon, conjugated synthetic polymer rayon, etc., can solve the problem of increasing the force between carbon atoms, low tensile strength and modulus, etc. problem, to achieve the effect of simple preparation method, good tensile strength and tensile modulus, excellent tensile strength and tensile modulus
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Embodiment 1
[0029] (1) Degrade and isomerize 65 parts of starch with 0.02 part of glucose isomerase and 0.01 part of amylase at 25°C for 4 hours to obtain product A;
[0030] (2) Add 1 part of ferric chloride and 1 part of copper chloride to product A, dehydrate at 105°C for 3 hours, separate and dry to obtain product B;
[0031] (3) After mixing the product B with 8 parts of paraffin, 4 parts of phthalic acid, 4 parts of oxalic acid, 15 parts of polyacrylonitrile, and 8 parts of vinyl silicone oil, use a twin-screw extruder to Carry out cross-linking polymerization reaction; obtain product C; the maximum temperature of the working area in the twin-screw extruder is set to 330°C, and the minimum temperature is set to 280°C; the residence time of the material in the extruder is controlled at 90s;
[0032] (4) Melt spinning the product C at a temperature of 330°C to obtain starch-based carbon fiber precursors;
[0033] (5) The starch-based carbon fiber precursors were subjected to the firs...
Embodiment 2
[0035] (1) Degrade and isomerize 50 parts of starch with 0.01 part of glucose isomerase and 0.01 part of amylase at 35°C for 5 hours to obtain product A;
[0036] (2) Add 1 part of ferrous chloride to product A, dehydrate at 85°C for 5 hours, separate and dry to obtain product B;
[0037] (3) Mix the product B with 5 parts of paraffin, 5 parts of hydroquinone, 5 parts of ethylene glycol, 20 parts of polyacrylonitrile, and 5 parts of vinyl silicone oil, and then use a twin-screw extruder to carry out extruding Copolymerization reaction; product C is obtained; the maximum temperature of the working area in the twin-screw extruder is set to 320°C, and the minimum temperature is set to 260°C; the residence time of the material in the extruder is controlled at 120s;
[0038] (4) Melt spinning the product C at a temperature of 350°C to obtain starch-based carbon fiber precursors;
[0039] (5) The starch-based carbon fiber precursors are subjected to the first pre-oxidation at 240°C...
Embodiment 3
[0041] (1) Degrade and isomerize 80 parts of starch with 0.03 parts of glucose isomerase and 0.02 parts of amylase at 35°C for 2 hours to obtain product A;
[0042] (2) Add 1 part of ferric chloride, 1 part of ferrous chloride and 1 part of hydrochloric acid to product A, dehydrate at 120°C for 1 hour, separate and dry to obtain product B;
[0043] (3) Mix product B with 10 parts of paraffin, 2 parts of ethylene glycol, 3 parts of glycerol, 10 parts of polyacrylonitrile, and 10 parts of vinyl silicone oil, and then use a twin-screw extruder to process Cross-linking polymerization reaction; product C is obtained; the maximum temperature of the working area in the twin-screw extruder is set to 340°C, and the minimum temperature is set to 290°C; the residence time of the material in the extruder is controlled at 60s;
[0044] (4) Melt spinning the product C at a temperature of 310°C to obtain starch-based carbon fiber precursors;
[0045] (5) The starch-based carbon fiber precurso...
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