Phenolic foam thermal-insulation material and preparation method thereof
A technology of thermal insulation material and phenolic foam, applied in the field of phenolic foam thermal insulation material and its preparation, can solve the problems of non-extensible water absorption, slightly poor thermal insulation performance, backward production technology, etc. low cost effect
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Embodiment 1
[0022] A phenolic foam insulation material, comprising the following raw materials by weight: 80 parts of phenolic resin; 10 parts of glass fiber; 3 parts of expandable graphite; 10 parts of silane coupling agent; 12 parts of foaming agent; and 9 parts of curing agent.
[0023] The glass fiber is a chopped glass fiber with a diameter of 10-20 microns and a length of 3-6 mm, which is made of glass balls or waste glass as raw materials through high temperature melting, wire drawing, winding, weaving and other processes.
[0024] The preparation method of the expandable graphite is as follows: using 50-mesh high-carbon flake graphite, concentrated sulfuric acid, potassium dichromate and hydrogen peroxide as raw materials, stirring continuously for 40 min under the condition of 40 DEG C, and washing with water until neutral after the reaction is completed, It was obtained by vacuum drying after centrifugation.
[0025] The silane coupling agent is vinyl silane; the foaming agent i...
Embodiment 2
[0028] A phenolic foam insulation material comprises the following raw materials by weight: 90 parts of phenolic resin; 15 parts of glass fiber; 4 parts of expandable graphite; 10 parts of silane coupling agent; 12 parts of foaming agent; and 10 parts of curing agent.
[0029] The glass fiber is a chopped glass fiber with a diameter of 10-20 microns and a length of 3-6 mm, which is made of glass balls or waste glass as raw materials through high temperature melting, wire drawing, winding, weaving and other processes.
[0030] The preparation method of the expandable graphite is as follows: using 50-mesh high-carbon flake graphite, concentrated sulfuric acid, potassium dichromate and hydrogen peroxide as raw materials, stirring continuously for 40 min under the condition of 40 DEG C, and washing with water until neutral after the reaction is completed, It was obtained by vacuum drying after centrifugation.
[0031] The silane coupling agent is methacryloxysilane; the foaming ag...
Embodiment 3
[0034] A phenolic foam insulation material comprises the following raw materials by weight: 85 parts of phenolic resin; 15 parts of glass fiber; 4 parts of expandable graphite; 10 parts of silane coupling agent; 10 parts of foaming agent; and 12 parts of curing agent.
[0035] The glass fiber is a chopped glass fiber with a diameter of 10-20 microns and a length of 3-6 mm, which is made of glass balls or waste glass as raw materials through high temperature melting, wire drawing, winding, weaving and other processes.
[0036] The preparation method of the expandable graphite is as follows: using 50-mesh high-carbon flake graphite, concentrated sulfuric acid, potassium dichromate and hydrogen peroxide as raw materials, stirring continuously for 40 min under the condition of 40 DEG C, and washing with water until neutral after the reaction is completed, It was obtained by vacuum drying after centrifugation.
[0037] The silane coupling agent is methacryloyloxysilane; the foaming...
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