Pasty thermal-conduction wave-absorbing electromagnetic material and preparation method thereof
An electromagnetic material and a paste-like technology are applied in the field of paste-like heat-conducting and wave-absorbing electromagnetic materials and their preparation, and can solve the problems of inability to achieve good heat dissipation effect, low thermal conductivity and magnetic permeability, poor thermal conductivity and wave-absorbing efficiency, and the like. To achieve the effect of improving the absorbing efficiency, good interface wettability and good absorbing effect
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[0041] The preparation method of the above-mentioned pasty heat-conducting and wave-absorbing electromagnetic material comprises the following steps:
[0042] 1) Add insulating and heat-conducting particles, electromagnetic absorbers and additives to the solvent, mix well, react at a constant temperature of 70-90°C for 1-10 hours, filter to remove the solvent, wash and dry the filtered solid to obtain heat-conducting wave-absorbing mixed powder body;
[0043] 2) Mix the silicone oil and the heat-conducting and wave-absorbing mixed powder evenly to obtain a paste;
[0044] 3) Grinding and dispersing the paste, performing densification and defoaming, to obtain a defoaming paste;
[0045] 4) Stir the defoaming paste in a vacuum state for 3-8 hours to obtain a paste-like heat-conducting and wave-absorbing electromagnetic material.
[0046] Preferably, the solvent described in step 1) is toluene, xylene, ethanol, isopropanol, pentane, hexane, octane, ether, propylene oxide, methy...
Embodiment 1
[0051] A paste-like heat-conducting and wave-absorbing electromagnetic material, the raw material composition of which is shown in the following table:
[0052] Table 1 The raw material composition list of a kind of pasty heat-conducting wave-absorbing electromagnetic material
[0053]
[0054]
[0055] The preparation method of the above-mentioned pasty heat-conducting and wave-absorbing electromagnetic material comprises the following steps:
[0056] 1) MgO powder, Fe-Si-Al-Ni alloy powder, dispersant, thickener, stabilizer, coupling agent and polymerization inhibitor are added to absolute ethanol (quality is Fe-Si-Al-Ni alloy powder quality 1.2 times of ), mixed evenly, reacted at a constant temperature of 70°C for 10 hours, filtered to remove absolute ethanol, washed and dried the filtered solid to obtain a heat-conducting and wave-absorbing mixed powder;
[0057] 2) Mix the simethicone oil and the heat-conducting and wave-absorbing mixed powder evenly to obtain a p...
Embodiment 2
[0061]A paste-like heat-conducting and wave-absorbing electromagnetic material, the raw material composition of which is shown in the following table:
[0062] Table 2 The raw material composition table of a kind of pasty heat-conducting wave-absorbing electromagnetic material
[0063] raw material
Mass percentage (%)
Simethicone oil (25℃, 5000cps)
28
AlN powder (D 50 : 4μm)
5
Permalloy powder (flaky, D 50 : 40μm)
65
Dispersant
1.5
coupling agent
0.5
[0064] The preparation method of the above-mentioned pasty heat-conducting and wave-absorbing electromagnetic material comprises the following steps:
[0065] 1) Add AlN powder, permalloy powder, dispersant and coupling agent to toluene (1.5 times the mass of permalloy powder), mix well, react at a constant temperature of 80°C for 5h, filter to remove toluene, and filter toluene The solid is washed and dried to obtain a heat-conducting and wave-absorbing mi...
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