The invention belongs to the technical field of electromagnetic wave-absorbing materials, and relates to a three-dimensional composite wave-absorbing material with Fe3O4 (at) C uniformly distributed on an MXene substrate, the material is of a three-dimensional
network structure, the three-dimensional
network structure forms a skeleton by carbon nanofibers, the skeleton is coated with MXene, and Fe3O4 is dispersed and distributed in the three-dimensional
network structure; the preparation method comprises the following steps: adding LiF and MAX into an acid solution for
etching, then washing, ultrasonically stripping and centrifuging to obtain single-layer MXene, preparing Fe3O4 microspheres by a hydrothermal method, adding the Fe3O4 microspheres and PAN into a DMF (
Dimethyl Formamide) solution, uniformly dispersing, then carrying out electrostatic
spinning, carbonizing in an
argon atmosphere, adding a surface-modified
spinning felt into the single-layer MXene solution, and
drying to obtain the product, a low-dimensional multi-stage coupled magnetic network and conductive network structure is formed, and meanwhile, the structure brings a large number of cavities and heterogeneous interfaces, so that incident electromagnetic
waves can be reflected for multiple times in the material, and the
electromagnetic wave absorption capacity is greatly improved.