New material for preparing clean hydrogen energy and preparation method of new material
A new material and hydrogen energy technology, applied in the field of new materials prepared by clean hydrogen energy and its preparation, can solve the problems of low hydrogen production rate, narrow photoresponse range, poor stability, etc., and achieve high photocatalytic activity and good repeatability , the effect of wide response range
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Embodiment 1
[0028] A new material for the preparation of clean hydrogen energy, comprising the following steps:
[0029] (1) Add 0.23g Zn(Ac) 2 2H 2 O, 0.3gIn(NO 3 ) 3 1. Add 0.6g of cerium nitrate to 100ml of ethanol solution, stir for 45min at a temperature of 70°C, then add 0.03g of thioacetamide, and continue stirring for 2h before use;
[0030] (2) Under constant stirring, add 50ml of 2mg / mL graphene oxide solution to the solution in step (1), and after stirring for 60min, transfer the resulting mixture to the reactor, react at a temperature of 160°C for 18h, and stop the reaction Afterwards, the reactor was cooled to room temperature, washed with water until neutral to obtain product A;
[0031] (3) Add 0.3g In(NO 3 ) 3 , 0.23g Cd(Ac) 2 2H 2 O. Add 0.6 g of cerium nitrate to 100 ml of ethanol solution, stir for 40 min at a temperature of 80° C., then add 0.03 g of thioacetamide, and continue stirring for 2 h for later use;
[0032] (4) Under constant stirring, add 50ml of 2...
Embodiment 2
[0035] A new material for the preparation of clean hydrogen energy, comprising the following steps:
[0036] (1) Add 0.23g Zn(Ac) 2 2H 2 O, 0.32gIn(NO 3 ) 3 1. Add 0.65g of cerium nitrate to 100ml of ethanol solution, stir for 45min at a temperature of 70°C, then add 0.05g of thioacetamide, and continue stirring for 2h before use;
[0037] (2) Under constant stirring, add 60ml of 2 mg / mL graphene oxide solution to the solution in step (1), stir for 60 minutes, transfer the resulting mixture to a reaction kettle, react at a temperature of 180°C for 15 hours, and stop the reaction Afterwards, the reactor was cooled to room temperature, washed with water until neutral to obtain product A;
[0038] (3) Add 0.32g In(NO 3 ) 3 , 0.23g Cd(Ac) 2 2H 2 O. Add 0.65 g of cerium nitrate to 100 ml of ethanol solution, stir for 40 min at a temperature of 80° C., then add 0.05 g of thioacetamide, and continue stirring for 2 h for later use;
[0039] (4) Under constant stirring, add 60...
Embodiment 3
[0042] A new material for the preparation of clean hydrogen energy, comprising the following steps:
[0043] (1) Add 0.3g Zn(Ac) 2 2H 2 O, 0.4gIn(NO 3 ) 3 1. Add 0.7g of cerium nitrate to 100ml of ethanol solution, stir for 45min at a temperature of 70°C, then add 0.06g of thioacetamide, and continue stirring for 2h before use;
[0044] (2) Under constant stirring, add 80ml of 2 mg / mL graphene oxide solution to the solution in step (1), stir for 60 minutes, transfer the resulting mixture to a reaction kettle, react at a temperature of 160°C for 18 hours, and stop the reaction Afterwards, the reactor was cooled to room temperature, washed with water until neutral to obtain product A;
[0045] (3) Add 0.4g In(NO 3 ) 3 , 0. 3g Cd(Ac) 2 2H 2 O. Add 0.7 g of cerium nitrate to 100 ml of ethanol solution, stir for 40 min at a temperature of 80° C., then add 0.06 g of thioacetamide, and continue stirring for 2 h for later use;
[0046] (4) Under constant stirring, add 80ml of...
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