Preparation method of diatom ooze special for walls
A diatom mud and wall technology, applied in the field of building materials, can solve problems such as poor bonding strength of diatom mud, and achieve the effects of enhancing bonding strength, enhancing activity, and reducing pore channels
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example 1
[0028]Add peach gum and water to the No. 1 beaker at a mass ratio of 1:60, stir and mix with a glass rod for 30 minutes, let it stand for swelling for 4 hours, and then move the beaker into a magnetic stirrer with a digital speed measurement and constant temperature at a temperature of 40°C and a speed of 500r Under the condition of heating and stirring for 40 min, the peach gum solution is obtained; in parts by weight, 20 parts of sulfuric acid with a mass fraction of 80% and 30 parts of 30% hydrogen peroxide with a mass fraction of 30% are taken successively, and then the mass fraction is 80% % sulfuric acid was added in the four-necked flask, and the mass fraction was added dropwise to the four-necked flask with a constant pressure dropping funnel at a rate of 2.5mL / min, and the mass fraction was 30% hydrogen peroxide, and at a rotating speed of 400r / min, it was added dropwise while stirring, After the mass fraction of 30% hydrogen peroxide is added dropwise, stir and mix fo...
example 2
[0030] Add peach gum and water to the No. 1 beaker at a mass ratio of 1:60, stir and mix with a glass rod for 30 minutes, let it stand for swelling for 4 hours, and then move the beaker into a magnetic stirrer with a digital speed measurement and constant temperature at a temperature of 40°C and a speed of 500r Under the condition of heating and stirring for 40 min, the peach gum solution is obtained; in parts by weight, 20 parts of sulfuric acid with a mass fraction of 80% and 30 parts of 30% hydrogen peroxide with a mass fraction of 30% are taken successively, and then the mass fraction is 80% % sulfuric acid was added in the four-necked flask, and the mass fraction was added dropwise to the four-necked flask with a constant pressure dropping funnel at a rate of 2.5mL / min, and the mass fraction was 30% hydrogen peroxide, and at a rotating speed of 400r / min, it was added dropwise while stirring, After the mass fraction of 30% hydrogen peroxide is added dropwise, under the cond...
example 3
[0032] Add peach gum and water to the No. 1 beaker at a mass ratio of 1:60, stir and mix with a glass rod for 30 minutes, let it stand for swelling for 4 hours, and then move the beaker into a magnetic stirrer with a digital speed measurement and constant temperature at a temperature of 40°C and a speed of 500r Under the condition of heating and stirring for 40 minutes, the peach gum solution is obtained; diatomite and peach gum solution are added into the No. 2 flask according to the mass ratio of 1:100, and the No. 2 beaker is moved to the ultrasonic disperser, and the frequency is Under the condition of 60kHz, ultrasonically disperse for 40 minutes to obtain a dispersion; filter the obtained dispersion to obtain a filter residue; place the obtained filter residue in a carbonization furnace, and pass nitrogen gas into the furnace at a rate of 90mL / min, at a temperature of 550°C , under the condition of nitrogen protection, heat preservation and carbonization for 3 hours, and ...
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