Functional shampoo

[0027] Example 1

[0028] Place the sponge in a sponge pulverizer and smash it through a 50-mesh sieve to obtain sponge powder; place the silkworm chrysalis and water in a juicer at a mass ratio of 1:20, and squeeze the juice to obtain silkworm pupa pulp juice; in parts by weight, in order Take 30 parts of 30% by mass ferric chloride solution, 20 parts of sponge powder, 0.2 parts of 10% by mass hydrochloric acid, 20 parts of 30% by mass ammonia water, and 30% by mass of ferric chloride solution , Sponge powder, 10% hydrochloric acid in the No. 1 beaker, stir and mix for 30 minutes at a speed of 400r/min, and then filter the mixture to obtain a filter residue. Place the resulting filter residue in Ammonia water with a mass fraction of 30% was stirred and mixed for 30 minutes at a speed of 400r/min and filtered to obtain a reaction solution. Then the reaction solution was filtered to obtain a filter cake, and then the filter cake was placed in a muffle furnace to The heating rate is 6°C/min to 650°C, calcined at a temperature of 650°C for 60 minutes and then down to room temperature to obtain massage beads; add chitosan to water at a mass ratio of 1:100 into No. 2 beaker After stirring and mixing with a glass rod for 30 minutes, let it stand and swell for 4 hours, and then move the No. 2 beaker into a digital display speed constant temperature magnetic stirrer. At a temperature of 100°C and a rotation speed of 500r/min, heat and stir to dissolve for 60 minutes. Chitosan liquid: Place the massage beads and the dopamine solution with a mass concentration of 2g/L in a No. 3 beaker at a mass ratio of 1:100, stir and mix and soak for 60 minutes at a speed of 400r/min to obtain the soaking liquid. Filter the soaking liquid to obtain pretreated massage beads; in parts by weight, place 30 parts of pretreated massage beads, 10 parts of oil, 0.2 parts of lipase, 6 parts of keratin, and 0.2 parts of keratinase in a No. 4 beaker, Under the condition of 400r/min, stir, mix and soak for 60min. After stirring and mixing, filter to obtain one-time treatment massage beads; put the one-time treatment massage beads and chitosan liquid in a No. 5 beaker at a rotation speed of 400r/min Under conditions, stir and mix for 50 minutes to obtain a mixed slurry, then place the mixed slurry in a refrigerator and freeze for 3 hours at a temperature of -20°C to obtain a frozen block, and then place the frozen block at room temperature to thaw naturally. The freezing and thawing cycle is 10 times to obtain the thawing liquid, and the thawing liquid is filtered to obtain the modified massage beads; in parts by weight, 40 parts of surfactant, 4 parts of thickener, 4 parts of cosolvent, 2 parts 1 part preservative, 2 parts buffer, 2 parts essence, 2 parts pigment, 120 parts water, 20 parts modified massage beads, 6 parts silkworm chrysalis pulp juice are added to the mixer, and the speed is 1200r/min, high-speed stirring Mix for 50 minutes to get a functional shampoo. The surfactant is sodium dodecylbenzene sulfonate. The thickener is ammonium chloride. The co-solvent is propylene glycol. The preservative is methyl paraben. The buffer is citric acid. The fragrance is lemon scent. The pigment is lemon yellow.

[0029] Example 2

[0030] Place the sponge in a sponge pulverizer and smash it through a 50-mesh sieve to obtain sponge powder; place the silkworm chrysalis and water in a juicer at a mass ratio of 1:20, and squeeze the juice to obtain silkworm pupa pulp juice; in parts by weight, in order Take 30 parts of 30% by mass ferric chloride solution, 20 parts of sponge powder, 0.2 parts of 10% by mass hydrochloric acid, 20 parts of 30% by mass ammonia water, and 30% by mass of ferric chloride solution , Sponge powder, 10% hydrochloric acid in the No. 1 beaker, stir and mix for 30 minutes at a speed of 400r/min, and then filter the mixture to obtain a filter residue. Place the resulting filter residue in Ammonia water with a mass fraction of 30% was stirred and mixed for 30 minutes at a speed of 400r/min and filtered to obtain a reaction solution. Then the reaction solution was filtered to obtain a filter cake, and then the filter cake was placed in a muffle furnace to The heating rate is 6°C/min to 650°C, calcined at a temperature of 650°C for 60 minutes and then down to room temperature to obtain massage beads; add chitosan to water at a mass ratio of 1:100 into No. 2 beaker After stirring and mixing with a glass rod for 30 minutes, let it stand and swell for 4 hours, and then move the No. 2 beaker into a digital display speed constant temperature magnetic stirrer. At a temperature of 100°C and a rotation speed of 500r/min, heat and stir to dissolve for 60 minutes. Chitosan liquid; in parts by weight, mix 40 parts of surfactant, 4 parts of thickener, 4 parts of cosolvent, 2 parts of preservative, 2 parts of buffer, 2 parts of flavor, 2 parts of pigment, 120 parts of water , 20 parts of massage beads, 6 parts of silkworm chrysalis pulp juice are added to the blender, and mixed at high speed for 50 minutes under the condition of rotating speed of 1200r/min to obtain functional shampoo. The surfactant is sodium dodecylbenzene sulfonate. The thickener is ammonium chloride. The co-solvent is propylene glycol. The preservative is methyl paraben. The buffer is citric acid. The fragrance is lemon scent. The pigment is lemon yellow.

[0031] Example 3

[0032] In parts by weight, take 30 parts of 30% ferric chloride solution, 20 parts of sponge powder, 0.2 parts of 10% hydrochloric acid, 20 parts of 30% ammonia water, and set the mass fraction to Place 30% ferric chloride solution, sponge powder, and 10% hydrochloric acid in a No. 1 beaker, stir and mix for 30 minutes at a speed of 400r/min, and then filter the mixture to obtain a filter residue , Then place the obtained filter residue in 30% ammonia water, stir and mix for 30 minutes at a speed of 400r/min, and filter to obtain a reaction solution. Then the reaction solution is filtered to obtain a filter cake, and then the filter cake is placed In a muffle furnace, heat up to 650°C at a heating rate of 6°C/min. Calcinate at a temperature of 650°C for 60 minutes at a high temperature and then drop to room temperature to obtain massage beads. The chitosan and water are mass ratioed. 1:100 was added to the No. 2 beaker, stirred and mixed with a glass rod for 30 minutes, then allowed to stand to swell for 4 hours, and then the No. 2 beaker was moved into the digital display speed measuring constant temperature magnetic stirrer, at a temperature of 100°C and a rotation speed of 500r/min. Heat and stir to dissolve for 60 minutes to obtain chitosan liquid; put the massage beads and the dopamine solution with a mass concentration of 2g/L in a No. 3 beaker at a mass ratio of 1:100, and stir, mix and soak at a speed of 400r/min 60min, get the soaking liquid, and then filter the soaking liquid to get pretreated massage beads; in parts by weight, 30 parts of pretreated massage beads, 10 parts of oil, 0.2 parts of lipase, 6 parts of keratin, 0.2 parts of keratinase Place it in the No. 4 beaker, stir, mix and soak for 60 minutes at a speed of 400r/min. After stirring and mixing, filter to obtain one-time treatment massage beads; place the one-time treatment massage beads and chitosan liquid in No. 5 beaker , At a speed of 400r/min, stir and mix for 50 minutes to obtain a mixed slurry, then place the mixed slurry in a refrigerator, and freeze for 3 hours at a temperature of -20°C to obtain a frozen block, and then place the frozen block Thaw naturally at room temperature, so freeze and thaw cycles 10 times to obtain thawing liquid, and filter the thawing liquid to obtain modified massage beads; in parts by weight, add 40 parts of surfactant and 4 parts of thickener , 4 parts co-solvent, 2 parts preservative, 2 parts buffering agent, 2 parts flavor, 2 parts pigment, 120 parts water, 20 parts modified massage beads are added to the mixer, at a speed of 1200r/min, high speed Stir and mix for 50 minutes to obtain a functional shampoo. The surfactant is sodium dodecylbenzene sulfonate. The thickener is ammonium chloride. The co-solvent is propylene glycol. The preservative is methyl paraben. The buffer is citric acid. The fragrance is lemon scent. The pigment is lemon yellow.