Preparation method of molecularly imprinted composite membrane material for selective recognition and separation of enoxacin
A technology of enoxacin and molecular imprinting, applied in semi-permeable membrane separation, chemical instruments and methods, membrane technology, etc., can solve problems such as environmental biological and ecological impact, adverse impact on human health and survival, etc. More spots, fast adsorption kinetics, improved hydrophilicity
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Embodiment 1
[0045] (1) Synthesis of polydopamine-modified multi-walled carbon nanotubes
[0046] Polydopamine-modified multi-walled carbon nanotubes were synthesized based on the biomimetic principle of dopamine. Disperse dopamine in the tris buffer solution, adjust the pH until it dissolves and changes color, put the multi-walled carbon nanotubes into the mixed solution, stir at room temperature for 3 hours, and fully react, so that the polydopamine layer is evenly wrapped in the polydopamine layer. nanotube surface. After the reaction, the obtained product was centrifuged, washed several times with deionized water to remove unreacted substances, and dried in vacuum for use.
[0047] (2) Preparation of enoxacin molecularly imprinted polymer
[0048] First, disperse 0.3mmol of enoxacin and 0.2ml of 3-aminopropyltriethoxysilane (APTES) in 30ml of ethanol solution and stir for 30 minutes; add a certain amount of tetraethyl silicate (TEOS) Continue stirring for 15 minutes; add ammonia wat...
Embodiment 2
[0061] (1) Synthesis of polydopamine-modified multi-walled carbon nanotubes
[0062] Polydopamine-modified multi-walled carbon nanotubes were synthesized based on the biomimetic principle of dopamine. Disperse dopamine in the tris buffer solution, adjust the pH until it dissolves and changes color, put the multi-walled carbon nanotubes into the mixed solution, stir at room temperature for 12 hours, and fully react, so that the polydopamine layer is evenly wrapped in the polydopamine layer. nanotube surface. After the reaction, the obtained product was centrifuged, washed several times with deionized water to remove unreacted substances, and dried in vacuum for use.
[0063] (2) Preparation of enoxacin molecularly imprinted polymer
[0064] First, disperse 0.5mmol of enoxacin and 0.2ml of 3-aminopropyltriethoxysilane (APTES) in 30ml of ethanol solution and stir for 30 minutes; add a certain amount of tetraethyl silicate (TEOS) Continue stirring for 15 minutes; add ammonia wa...
Embodiment 3
[0077] (1) Synthesis of polydopamine-modified multi-walled carbon nanotubes
[0078] Polydopamine-modified multi-walled carbon nanotubes were synthesized based on the biomimetic principle of dopamine. Disperse dopamine in the tris buffer solution, adjust the pH until it dissolves and changes color, put the multi-walled carbon nanotubes into the mixed solution, stir at room temperature for 8 hours, and fully react, so that the polydopamine layer is evenly wrapped in the polydopamine layer. nanotube surface. After the reaction, the obtained product was centrifuged, washed several times with deionized water to remove unreacted substances, and dried in vacuum for use.
[0079] (2) Preparation of enoxacin molecularly imprinted polymer
[0080] First, disperse 0.4mmol of enoxacin and 0.2ml of 3-aminopropyltriethoxysilane (APTES) in 30ml of ethanol solution and stir for 30 minutes; add a certain amount of tetraethyl silicate (TEOS) Continue to stir for 15 minutes; add ammonia wate...
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