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Process for lattice preparation of microcrystalline glass applied to 5G communication mobile terminals

A technology of glass-ceramics and mobile terminals, which is applied in glass manufacturing equipment, manufacturing tools, glass molding, etc., can solve problems such as no one involved, and achieve the effect of avoiding glass crystallization and reasonable temperature system

Active Publication Date: 2018-09-28
GLASS TECH RES INST OF SHAHE CITY OF HEBEI PROVINCE
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

However, the process of producing high-strength glass-ceramics by Gefa has not been involved yet.

Method used

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  • Process for lattice preparation of microcrystalline glass applied to 5G communication mobile terminals

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0035] A method for preparing glass-ceramics for 5G communication mobile terminals, the preparation process is as follows:

[0036]A. First, the raw materials are accurately weighed according to the material recipe, and the batches that are forced to mix evenly are put into the feeding pool at regular intervals and quantitatively. The ingredients are as follows: 50 parts of quartz sand, 10.5 parts of alumina, 15 parts of sodium carbonate, 2.5 parts of potassium nitrate, 2 parts of lithium carbonate, 9.5 parts of magnesium oxide, 3 parts of titanium oxide, 2.5 parts of zirconia, 4 parts of zinc oxide, 0.5 parts of rubidium, 0.25 parts of gallium oxide, and 0.25 parts of europium oxide.

[0037] B. The batch material in the melting pool is heated to 1525°C for melting, clarified, stirred and homogenized to obtain a high-quality defect-free molten glass.

[0038] C. Grating method forming: the above-mentioned molten glass is vertically drawn above the lead brick to form, and the...

Embodiment 2

[0044] A. First, the raw materials are accurately weighed according to the material recipe, and the batches that are forced to mix evenly are put into the feeding pool at regular intervals and quantitatively. The ingredients are as follows: 50 parts of quartz sand, 15.5 parts of alumina, 26.3 parts of sodium carbonate, 4.6 parts of potassium nitrate, 13.3 parts of magnesium oxide, and 4.45 parts of ammonium dihydrogen phosphate.

[0045] B. The batch material in the melting pool is heated to 1500°C for melting, clarified, stirred and homogenized to obtain a high-quality defect-free molten glass.

[0046] C. Grating method forming: the above-mentioned molten glass is vertically drawn above the lead brick to form, and the forming temperature is controlled to be 1000°C. , 18.5mm / s.

[0047] D. When the glass ribbon is cooled to 650°C, enter the annealing kiln for annealing, nucleate at 680°C for 2 hours, and crystallize at 800°C for 2 hours to obtain the original glass ceramics....

Embodiment 3

[0051] A. First, the raw materials are accurately weighed according to the material recipe, and the batches that are forced to mix evenly are put into the feeding pool at regular intervals and quantitatively. The ingredients are as follows: 48.2 parts of quartz sand, 20.6 parts of alumina, 24.5 parts of sodium carbonate, 2.3 parts of potassium nitrate, 10.6 parts of lithium carbonate, 7.5 parts of magnesium oxide, 2 parts of zirconia, 1.55 parts of ammonium dihydrogen phosphate, and 1 part of antimony oxide , 1 part of rubidium oxide.

[0052] B. The batch materials in the melting pool are heated to 1550°C for melting, clarified, stirred and homogenized to obtain a high-quality defect-free molten glass.

[0053] C. Grating method forming: the above-mentioned molten glass is vertically drawn above the leading brick to form, and the forming temperature is controlled to be 1016°C. Speed ​​20mm / s.

[0054] D. When the glass ribbon is cooled to 600°C, enter the annealing kiln for...

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Abstract

The invention belongs to the technical field of microcrystalline glass and discloses a process for lattice preparation of microcrystalline glass applied to 5G communication mobile terminals. The process includes steps: A, raw material preparation, namely preparing, by weight, 45-75 parts of quartz sand, 10-25 parts of aluminum oxide, 14.5-39.6 parts of sodium carbonate, 2.3-9.2 parts of potassiumnitrate, 0-12.5 parts of lithium carbonate, 0-20 parts of magnesium oxide, 0-8 parts of titanium oxide, 0-20 parts of zirconium oxide, 0-10 parts of zinc oxide, 0-9 parts of ammonium dihydrogen phosphate, 0-3 parts of antimony oxide, 0-3 parts of europium oxide and 0-5 parts of ferric oxide, and mixing to obtain a batch mixture; B, glass melting; C, lattice formation; D, glass annealing, nucleating and crystallizing, and chemically strengthening to obtain the microcrystalline glass applied to the 5G communication mobile terminals. The microcrystalline glass prepared according to the process has excellent optical and mechanical performances, is free of surface defects such as brush lines and stripes and can be applied to electronic terminal display protection screens and rear cover protection shells.

Description

technical field [0001] The invention belongs to the technical field of glass-ceramics, and in particular relates to a glass-ceramics lattice method preparation process applied to 5G communication mobile terminals. Background technique [0002] In the field of communication mobile terminal electronic equipment, chemically strengthened glass is often used as a screen protection material. However, although traditional chemically strengthened glass is scratch-resistant and scratch-resistant, it still cannot resist the impact caused by falling equipment. Moreover, with the development of 5G signals, the metal materials usually used for the back cover of mobile terminals are also restricted to a certain extent. [0003] As a kind of glass material, glass-ceramics can obtain higher mechanical properties than amorphous glass through compositional design and controlled crystallization. At the same time, reasonable chemical strengthening can be used to enhance the drop impact resista...

Claims

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Application Information

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IPC IPC(8): C03C6/04C03B15/08C03B25/00C03B32/02C03C21/00
CPCC03B15/08C03B25/00C03B32/02C03C1/00C03C21/002
Inventor 杜晓欧袁坚郑伟宏田培静彭志钢史连莹张茂森刘皓
Owner GLASS TECH RES INST OF SHAHE CITY OF HEBEI PROVINCE