Super-hydrophobic nano-fiber composite membrane for membrane distillation and preparation method thereof
A nanofiber and composite membrane technology, applied in the field of material engineering, can solve the problems of increasing the preparation cost of membrane distillation membranes, hindering the popularization and application of membrane distillation technology, and expensive hydrophobic modifiers. The preparation method is simple and easy to operate, and the price is low.
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Embodiment 1
[0026] A preparation method of superhydrophobic nanofiber composite membrane for membrane distillation:
[0027] (1) 15 g of polyvinylidene fluoride (PVDF) was dissolved in 85 g of N,N-dimethylformamide (DMF), and stirred at a constant temperature in an oil bath at 80° C. for 24 hours to obtain a uniform and transparent electrospinning solution. Dissolve 0.3 g of atactic polypropylene in 99.7 g of xylene, stir in an oil bath at 99°C for 5 hours at a constant temperature to obtain a uniform and transparent suction-filtered solution, and then cool it to 60°C at 30°C for use;
[0028] (2) Add the electrospinning stock solution in (1) into the container, and control the extrusion rate by a micro-injection pump. The extrusion rate of the solution is 5 μL / min. The relative humidity is 36%, the ambient temperature is 31°C, the rotating speed of the receiving drum is 800r / min, and electrospinning is performed, the average diameter of the obtained polyvinylidene fluoride electrospun na...
Embodiment 2
[0033] A preparation method of superhydrophobic nanofiber composite membrane for membrane distillation:
[0034] (1) Dissolve 20 g of poly(vinylidene fluoride-co-hexafluoropropylene) in 80 g of N,N-dimethylacetamide as a spinning solution, and stir it in an oil bath at 40°C for 24 hours to obtain a uniform Transparent electrospinning solution. Dissolve 0.3 g of polyethylene in 99.7 g of xylene, stir in an oil bath at 99°C for 5 hours at a constant temperature to obtain a uniform and transparent suction-filtered solution, and then cool it to 50°C at 30°C for later use;
[0035] (2) Add the electrospinning stock solution in (1) into the container respectively, and control the extrusion rate by a micro-injection pump, the solution extrusion rate is 5 μL / min, the eccentric needle is connected to a high-voltage electrode, the voltage is 25kV, and the receiving distance is 15cm , air relative humidity is 32%, ambient temperature is 30 ℃, and receiving drum rotating speed is 700r / mi...
Embodiment 3
[0040] A preparation method of superhydrophobic nanofiber composite membrane for membrane distillation:
[0041] (1) 8 g of polyacrylonitrile was dissolved in 92 g of N,N-dimethylformamide, and stirred at a constant temperature in an oil bath at 50° C. for 6 h to obtain a uniform and transparent electrospinning solution. Dissolve 0.6 g of atactic polypropylene in 99.4 g of cyclohexane, stir in an oil bath at 95°C for 5 hours at a constant temperature to obtain a uniform and transparent suction-filtered solution, and then cool it to 30°C at 20°C for use;
[0042] (2) Add the electrospinning stock solution in (1) into the container, and the extrusion rate is controlled by a micro-injection pump. The extrusion rate of the solution is 16 μL / min. The relative humidity is 36%, the ambient temperature is 31°C, the rotating speed of the receiving drum is 800r / min, and electrospinning is carried out, the average diameter of the obtained polyacrylonitrile electrospun nanofibers is 250nm...
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