Preparation method of biomass liquefied fuel oil

A biomass and fuel oil technology, which is applied in the preparation of liquid hydrocarbon mixtures and the petroleum industry, can solve environmental pollution and other problems, and achieve the effects of improving catalytic efficiency, increasing looseness, and increasing carbon content

Inactive Publication Date: 2018-12-21
FOSHAN WANHE NEW ENERGY TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] The technical problem to be solved by the present invention: Aiming at the problem that salt or alkali is often used as a catalyst in the process of pr

Method used

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  • Preparation method of biomass liquefied fuel oil

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preparation example Construction

[0025] A preparation method of biomass liquefied fuel oil, the preparation method comprising the steps of:

[0026] (1) Mix the raw materials, additives and water evenly according to the mass ratio of 6~7:1:3~5, steam explosion, set the pressure at 1~3MPa, maintain the pressure for 70s, collect the steam explosion, filter, collect the filter residue, and put Squeeze the filter residue at 4MPa for 30s, then put it into a loose machine to break up, and collect the broken matter;

[0027] (2) Soak the scattered matter in acetic acid solution for 2 hours according to the mass ratio of 1:3~5, filter, wash until neutral, collect the washings, count by weight parts, take 30~40 parts of washings, 120~ 130 parts of water, 7 to 9 parts of ferric sulfate, 6 to 8 parts of additives, placed in a container for ultrasonic vibration for 20 minutes;

[0028] (3) After the ultrasonic vibration is finished, add the mixed liquid in an amount of 30-32% of the water quality, heat to 40-45°C, stir ...

Embodiment 1

[0031] The raw material is to mix wheat stalks, corn stalks and sawdust evenly in a mass ratio of 3:5:9, put them into a pulverizer for crushing, and collect the crushed materials to obtain the raw materials.

[0032] The additive is mixed with ammonium bicarbonate and sodium bicarbonate at a mass ratio of 5:1.

[0033] The auxiliary agent is mixed with manganese sulfate and nickel nitrate in a mass ratio of 6:1.

[0034] The mixed solution is prepared by mixing sucrose and ammonium oxalate solution at a mass ratio of 4:20.

[0035] The mixed solution is formed by mixing methanol solution and acetone at a volume ratio of 5:4.

[0036] A preparation method of biomass liquefied fuel oil, the preparation method comprising the steps of:

[0037] (1) Mix the raw materials, additives, and water evenly according to the mass ratio of 7:1:5, steam explosion, set the pressure at 3MPa, maintain the pressure for 70s, collect the steam explosion, filter, collect the filter residue, and s...

Embodiment 2

[0042] The raw material is to mix wheat stalks, corn stalks and sawdust evenly in a mass ratio of 2:3:7, put them into a pulverizer for crushing, and collect the crushed materials to obtain the raw materials.

[0043] The additive is mixed with ammonium bicarbonate and sodium bicarbonate at a mass ratio of 4:1.

[0044] The auxiliary agent is mixed with manganese sulfate and nickel nitrate in a mass ratio of 5:1.

[0045] The mixed solution is prepared by mixing sucrose and ammonium oxalate solution at a mass ratio of 3:15.

[0046] The mixed solution is formed by mixing methanol solution and acetone at a volume ratio of 4:4.

[0047] A preparation method of biomass liquefied fuel oil, the preparation method comprising the steps of:

[0048] (1) Mix the raw materials, additives, and water evenly according to the mass ratio of 6.5:1:4, steam explosion, set the pressure at 2MPa, maintain the pressure for 70s, collect the steam explosion, filter, collect the filter residue, and s...

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Abstract

The invention belongs to the technical field of new energy, and in particular relates to a preparation method of biomass liquefied fuel oil. According to the preparation method, the raw materials arefirstly processed: the raw materials are firstly mixed with an additive, and steam blasting is performed, the looseness of the raw materials is improved by treating with the steam explosion, and the porosity of the raw materials is improved by the effect of the additive; and then the raw materials are soaked with acetic acid, so that micropores and cracks can be formed inside the raw materials bysoaking in acetic acid; next the raw materials are mixed with iron sulfate and an auxiliary agent, so that the metal ions in the system can be sedimented by the effect of the mixed liquor to fill thepores in the raw materials, thereby forming a state of the iron-manganese-nickel three elements wrapping raw materials, and improving the catalytic efficiency of the raw material; meanwhile, the addedsucrose can effectively increase the carbon content of the raw materials and promote the liquefaction efficiency; and finally, in the liquefaction process, preheating can be performed to firstly improve the activity of the raw materials, and the liquefied fuel oil is obtained after the liquefaction at high temperature and high pressure.

Description

technical field [0001] The invention belongs to the technical field of new energy, and in particular relates to a preparation method of biomass liquefied fuel. Background technique [0002] With the rapid development of science and technology, the development of biomass energy will rely on innovative technologies to achieve greater development. The new technology of biomass energy, especially the research on rapid liquefaction of atmospheric pressure to produce liquefied oil, once a breakthrough is made, will greatly promote the development and application of biomass energy, especially in remote rural areas. Liquefied into "biological crude oil" that is convenient for transportation and rich in industrial processing value, the long geochemical process is concentrated in tens of minutes. [0003] The advantage of the atmospheric pressure liquefaction method of biomass is that it can produce a thermochemical reaction of biomass resources with a solvent medium at a lower tempe...

Claims

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Application Information

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IPC IPC(8): C10G1/00
CPCC10G1/002
Inventor 裘友玖付平
Owner FOSHAN WANHE NEW ENERGY TECH CO LTD
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