Concrete release agent and preparation method thereof
A technology of concrete release agent and defoamer, which is applied in the field of concrete admixtures, can solve the problems of concrete surface damage, unfavorable mass production, poor release effect, etc., and achieve improved film-forming compactness, good dispersion and release and emulsification, to ensure the effect of aesthetic appearance
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Embodiment 1
[0027] A concrete release agent, made from the following raw materials and weight ratios: 10 parts of fluorine-containing linoleic acid compounds, 20 parts of modified vinyl fluorosilicone oil, 3 parts of dinonylphenol polyether-7-phosphate, 3 parts of N-[3-(2-furyl)acryloyl]-L-phenylalanyl-glycyl-glycine, 1 part of emulsifier OP-10, 15 parts of montmorillonite, hexadecyl trimethyl 1 part of ammonium chloride, 1 part of tributyl phosphate, and 65 parts of water; the fluorine-containing linoleic acid compound is prepared by Diels-Alder reaction of linoleic acid and perfluorobutadiene.
[0028] The preparation method of the modified vinyl fluorosilicone oil comprises the following steps: under a nitrogen atmosphere, mix 30 g of vinyl fluorosilicone oil with 2,2',2"-nitrilotris(ethoxy)(butadiene- 10g of 1,3-dien-2-yl)silane was added to a three-necked flask equipped with a reflux condenser and an electric stirrer, and 150g of isopropanol was added to the bottle, and the reaction ...
Embodiment 2
[0032] A concrete release agent, made of the following raw materials and weight ratios: 13 parts of fluorine-containing linoleic acid compounds, 23 parts of modified vinyl fluorosilicone oil, 4 parts of dinonylphenol polyether-7-phosphate, N-[3-(2-furyl)acryloyl]-L-phenylalanyl-glycyl-glycine 4 parts, Tween 80 2 parts, montmorillonite 17 parts, octadecyl trimethyl chloride 2 parts of ammonium chloride, 2 parts of defoamer Deqian 3100, and 68 parts of water; the fluorine-containing linoleic acid compound is prepared by Diels-Alder reaction of linoleic acid and perfluorobutadiene.
[0033]The preparation method of the modified vinyl fluorosilicone oil comprises the following steps: under a helium atmosphere, mix 35 g of vinyl fluorosilicone oil with 2,2',2"-nitrilotris(ethoxy)(butadiene -1,3-dien-2-yl)silane 10g was added to a three-neck flask equipped with a reflux condenser and an electric stirrer, and then 170g of ethanol was added to the bottle, and the reaction was refluxed...
Embodiment 3
[0037] A concrete release agent, made from the following raw materials and weight ratios: 15 parts of fluorine-containing linoleic acid compounds, 25 parts of modified vinyl fluorosilicone oil, 5 parts of dinonylphenol polyether-7-phosphate, N-[3-(2-furyl)acryloyl]-L-phenylalanyl-glycyl-glycine 5 parts, Span 80 2 parts, montmorillonite 18 parts, hexadecyl trimethyl chloride 3 parts of ammonium chloride, 2 parts of defoamer BYK088, and 70 parts of water; the fluorine-containing linoleic acid compound is prepared by Diels-Alder reaction of linoleic acid and perfluorobutadiene.
[0038] The preparation method of the modified vinyl fluorosilicone oil comprises the following steps: under a neon gas atmosphere, mix 40 g of vinyl fluorosilicone oil with 2,2',2"-nitrilotris(ethoxy)(butadiene 10g of -1,3-dien-2-yl)silane was added to a three-necked flask equipped with a reflux condenser and an electric stirrer, and then 180g of acetone was added to the bottle, and the reaction was refl...
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