Concrete release agent and preparation method thereof

A technology of concrete release agent and defoamer, which is applied in the field of concrete admixtures, can solve the problems of concrete surface damage, unfavorable mass production, poor release effect, etc., and achieve improved film-forming compactness, good dispersion and release and emulsification, to ensure the effect of aesthetic appearance

Inactive Publication Date: 2018-12-21
HUNAN CHENLI NEW MATERIAL CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Traditional release agents are mostly made of engine oil or waste engine oil plus diesel. This type of release agent is easy to pollute the concrete surface and also cause pollution to the environment to varying degrees.
At present, the domestic release agents mainly include soap release agents, oil release agents, paraffin release agents and oil-based release agents, which generally have poor release effects, are difficult to remove after removal, and are easy to damage the concrete surface. Defects that cause damage, affect construction efficiency and increase construction costs
[0004] China Patent Office Patent Publication No. CN1021972C discloses the use of vegetable oil foot soap to produce mold release agents. Although it has the characteristics of non-toxicity and strong oiliness, the production cost is too high in actual production, which is not conducive to mass production.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] A concrete release agent, made from the following raw materials and weight ratios: 10 parts of fluorine-containing linoleic acid compounds, 20 parts of modified vinyl fluorosilicone oil, 3 parts of dinonylphenol polyether-7-phosphate, 3 parts of N-[3-(2-furyl)acryloyl]-L-phenylalanyl-glycyl-glycine, 1 part of emulsifier OP-10, 15 parts of montmorillonite, hexadecyl trimethyl 1 part of ammonium chloride, 1 part of tributyl phosphate, and 65 parts of water; the fluorine-containing linoleic acid compound is prepared by Diels-Alder reaction of linoleic acid and perfluorobutadiene.

[0028] The preparation method of the modified vinyl fluorosilicone oil comprises the following steps: under a nitrogen atmosphere, mix 30 g of vinyl fluorosilicone oil with 2,2',2"-nitrilotris(ethoxy)(butadiene- 10g of 1,3-dien-2-yl)silane was added to a three-necked flask equipped with a reflux condenser and an electric stirrer, and 150g of isopropanol was added to the bottle, and the reaction ...

Embodiment 2

[0032] A concrete release agent, made of the following raw materials and weight ratios: 13 parts of fluorine-containing linoleic acid compounds, 23 parts of modified vinyl fluorosilicone oil, 4 parts of dinonylphenol polyether-7-phosphate, N-[3-(2-furyl)acryloyl]-L-phenylalanyl-glycyl-glycine 4 parts, Tween 80 2 parts, montmorillonite 17 parts, octadecyl trimethyl chloride 2 parts of ammonium chloride, 2 parts of defoamer Deqian 3100, and 68 parts of water; the fluorine-containing linoleic acid compound is prepared by Diels-Alder reaction of linoleic acid and perfluorobutadiene.

[0033]The preparation method of the modified vinyl fluorosilicone oil comprises the following steps: under a helium atmosphere, mix 35 g of vinyl fluorosilicone oil with 2,2',2"-nitrilotris(ethoxy)(butadiene -1,3-dien-2-yl)silane 10g was added to a three-neck flask equipped with a reflux condenser and an electric stirrer, and then 170g of ethanol was added to the bottle, and the reaction was refluxed...

Embodiment 3

[0037] A concrete release agent, made from the following raw materials and weight ratios: 15 parts of fluorine-containing linoleic acid compounds, 25 parts of modified vinyl fluorosilicone oil, 5 parts of dinonylphenol polyether-7-phosphate, N-[3-(2-furyl)acryloyl]-L-phenylalanyl-glycyl-glycine 5 parts, Span 80 2 parts, montmorillonite 18 parts, hexadecyl trimethyl chloride 3 parts of ammonium chloride, 2 parts of defoamer BYK088, and 70 parts of water; the fluorine-containing linoleic acid compound is prepared by Diels-Alder reaction of linoleic acid and perfluorobutadiene.

[0038] The preparation method of the modified vinyl fluorosilicone oil comprises the following steps: under a neon gas atmosphere, mix 40 g of vinyl fluorosilicone oil with 2,2',2"-nitrilotris(ethoxy)(butadiene 10g of -1,3-dien-2-yl)silane was added to a three-necked flask equipped with a reflux condenser and an electric stirrer, and then 180g of acetone was added to the bottle, and the reaction was refl...

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PUM

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Abstract

The invention discloses a concrete release agent. The concrete release agent is prepared from the following raw materials in parts by weight: 10-20 parts of fluorine-containing linoleic acid compound,20-30 parts of modified vinyl fluorosilicone oil, 3-6 parts of dinonyl phenol polyether-7-phosphate, 3-6 parts of N-[3-(2-furyl)acryloyl]-L-phenylalanyl-glycyl-glycine, 1-3 parts of an emulsifier, 15-20 parts of montmorillonoid, 1-3 parts of a quaternary ammonium salt surfactant, 1-3 parts of a defoamer, and 65-75 parts of water; the fluorine-containing linoleic acid compound is prepared from linoleic acid and hexafluorobutadiene through Diels-Alder reaction. The invention also discloses a preparation method of the concrete release agent. The concrete release agent prepared by the preparationmethod has stable performance, good release effect and high release efficiency, can greatly reduce environmental pollution and material cost, and ensure appearance aesthetics of concrete members.

Description

technical field [0001] The invention relates to the technical field of concrete admixtures, in particular to a concrete release agent and a preparation method thereof. Background technique [0002] With the development of the economy and the advancement of urban-rural integration, high-rise buildings have sprung up like mushrooms after rain, and flat roads meander to the distance, presenting a modern urban-rural combination cityscape. Concrete is an indispensable common building material in the construction of these high-rise buildings, and mixed soil is a kind of building material with high plasticity, which can make the architect's architectural ideal into reality. During its construction, it is often necessary to use plates or special-shaped molds to support it first. Before injecting evenly mixed concrete raw materials into the mold, it is also necessary to brush a layer of concrete release agent on the inside of the mold and formwork to make it effective. Improve const...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C10M173/02B28B7/38C10N40/36C10N30/06C10N30/08C10N30/12C10N30/16
CPCB28B7/384B28B7/388C10M173/02C10M2201/103C10M2207/289C10M2209/103C10M2209/108C10M2211/044C10M2215/04C10M2215/08C10M2223/04C10M2225/04C10M2229/051C10N2030/06C10N2030/08C10N2030/12C10N2030/16C10N2040/36C10N2030/56
Inventor 万章文曹冰
Owner HUNAN CHENLI NEW MATERIAL CO LTD
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